Make Zinc Powder by Electrolysis

  Рет қаралды 177,149

NurdRage

NurdRage

8 жыл бұрын

We show how to make Zinc powder by electrochemistry.
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Пікірлер: 273
@smokecrackhailsatan
@smokecrackhailsatan 8 жыл бұрын
My favorite thing about this channel is the warning in the beginning doesn't end with "please don't try this at home", it ends with "wear gloves when handling".
@noodledoodle4655
@noodledoodle4655 6 жыл бұрын
Don't come running to me if you blow your leg off
@j1j250
@j1j250 5 жыл бұрын
Better tell people how to be safe rather then them do it without proper safety because they don’t know how to
@WeebRemover4500
@WeebRemover4500 5 жыл бұрын
@the rougemillenial yes they compensate by appearing authoritative, its quite childish really
@benjaminjustice2438
@benjaminjustice2438 2 жыл бұрын
you all prolly dont care but does anyone know of a trick to get back into an Instagram account?? I was stupid forgot my account password. I appreciate any tricks you can offer me
@nathanielmatthias9360
@nathanielmatthias9360 2 жыл бұрын
@Benjamin Justice Instablaster ;)
@VerbenaIDK
@VerbenaIDK 2 жыл бұрын
for anyone willing to make some zinc powder, and for some reason doenst have zinc oxide nearby but has d2 batteries, you can directly dissolve metal zinc in sodium hydroxide, just know that depending on the brand the battery internals changes, in my opinion, of you want to take it apart easily and have nice clean zinc case, rather than rayovac that gas some weird solic black glue that can be a pain to deal woth it since i have no idea what it is also, i measured the zinc body of the batteries i recently dissasembled, and my scale says both are 9 grams, that may change from battery from battery, brand from brand, but average i think it's not far off to suppose it would be around ~9 grams for most batteries from most brands if you for some reason dont want to wait to zonc oxide to arrive, have to make zinc oxide or have some zinc metal around and dont want to buy zinc oxide, i hope this helps! but if you really are in a hurry, i shouldnt have to mention but i will anyway: dissolving the zinc metal into solution will take a lot longer than fine zinc oxide powder! as a side note: as always, when reacting metals, clean it as best as you can, sand it all around, steel wool, steel brush as best as you can to make the reaction faster, the cleaner the faster it will react
@zahariburgess3660
@zahariburgess3660 2 ай бұрын
Thank you 🙏
@evanriddle1614
@evanriddle1614 3 жыл бұрын
I've made these dendrites and used them for air batteries. It works but the zinc powder dissolves like putting snow under a blow torch. This very thing is being used for power storage systems and was used by the German postal service to power their trucks but was only a pilot program that was discontinued. Thanks!
@noisytim
@noisytim 8 жыл бұрын
The tarnished zinc looks absolutely stunning. A high-resolution photo of that would make an amazing print or backdrop. Maybe even a wallpaper.
@rich1051414
@rich1051414 8 жыл бұрын
Zinc oxide will also fluoresce orange under a black light :)
@neurotoksin
@neurotoksin 8 жыл бұрын
Loving the 4K uploads! Looks great :D
@NurdRage
@NurdRage 8 жыл бұрын
I've purchased another hotplate stirrer so hopefully that will arrive soon. Then we can get back to real chemistry. (The hotplate stirrer in the video is another broken one that just stirs and doesn't heat)
@3Dusers
@3Dusers 8 жыл бұрын
how does it stir, a magnet? how does the magnet work
@3Dusers
@3Dusers 8 жыл бұрын
how does water get stirred with a magenet
@3Dusers
@3Dusers 8 жыл бұрын
oh there's a magnet inside the water that spins
@DirectorAntify
@DirectorAntify 8 жыл бұрын
Can't you use a heating mantle overtop of the stirrer as a makeshift hot plate?
@spudybugged199
@spudybugged199 8 жыл бұрын
it alse works with Al2O3?
@OriginalUnknown2
@OriginalUnknown2 8 жыл бұрын
Thank you, Mr. Rage!
@biowerks
@biowerks 8 жыл бұрын
glad to see you again!
8 жыл бұрын
I love these videos but my family start getting worried about "demonic voice talking science" from my room.
@danre2492
@danre2492 3 жыл бұрын
xdddddddd
@ungnhanvaoprofilecuatoi2191
@ungnhanvaoprofilecuatoi2191 3 жыл бұрын
ng miền nào vậy
@WilianMarangoni
@WilianMarangoni 8 жыл бұрын
great video, its possible make a video about through-hole PCB plating?
@kemarre
@kemarre 8 жыл бұрын
I don't got money but. Got appreciation. I appreciate your sharing your knowledge. Thanks.
@muizzy
@muizzy 8 жыл бұрын
Have you upgraded your camera? Video quality is great in this one!
@AlphaPowell7
@AlphaPowell7 8 жыл бұрын
Does this work with cadmium? I know it and zinc have a bit in common being in the same group. I have a source of cadmium hydroxide and would like to make the metal.
@evanriddle1614
@evanriddle1614 3 жыл бұрын
Deutsche post office used this method to generate/regenerate for zinc air batteries for a small fleet of trucks in 1995. A company in Canada is doing something similar for power storage. The bundepost could generate 100kg per hour but it took 750kg to fuel a truck for 200 miles carrying 2 metric tons. My question is, how do you rinse and preserve the powder so I can make my own zinc air batteries? Thank you so very much!
@vabbe71
@vabbe71 2 жыл бұрын
Can you please make a vidfeo when maufacturing Raney-nickel catalyst. It's a superior catalyst in organic chemistry and does the same job as Pt/C, Pd/C and PtO2 but to a fraction of the nobel catalyst's
@harun7826
@harun7826 5 жыл бұрын
thank for this video. can I make lead powder from lead oxide with same method_?
@macronautics
@macronautics 8 жыл бұрын
Hey, would you like to make a video where you synthetise menthol? I cannot find it anywhere and I thought it might be quite interesting.
@stephenjacks8196
@stephenjacks8196 4 жыл бұрын
Hardware store has "galvanizing" paint which I sprayed into beaker of naphtha (thinner) and the zinc powder was reactive with aryl chloride. I cheated by using an ultrasonic source to stimulate the slow zinc reaction. Sonication stimutates grignard start and really seams to help with multiphase reactions (e.g. conc NaHSO4, NaBr, MeOH > MeBr). We took a grinder to a welding "zinc" but powder was too oxidized needed activation.
@philip9487
@philip9487 8 жыл бұрын
awsome video man
@saikittang7450
@saikittang7450 8 жыл бұрын
Can I use a copper anode? Also, can I dissolve zinc casings from dead batteries to make the sodium zincate solution? After all, both zinc and zinc oxide dissolves in sodium hydroxide
@mustafahelmiamri6391
@mustafahelmiamri6391 Жыл бұрын
hello sir, can you make a tutorial for melting tin into powder... for tin paste. hope the sustenance is smooth and the channel is growing
@kedeesinabasa873
@kedeesinabasa873 3 жыл бұрын
Wow I love it thank you for video
@shelbysgarage5828
@shelbysgarage5828 4 жыл бұрын
Could I.use a zinc anode? and would that transfer zinc to the copper cathode?
@transgayatheistmarijuanasm803
@transgayatheistmarijuanasm803 8 жыл бұрын
can this zinc powder be used to carry out the clemmensen reduction?
@jasonvaughn4177
@jasonvaughn4177 4 жыл бұрын
This is an old video but much appreciated. Very cool, although would using ZnCl2 work as a substitute for the oxide? I have a bunch of ZnCl2 that I don’t have a use for and zinc powder is def something I have wanted to play with. Great work as always 👍🏻
@gazzarrr666
@gazzarrr666 3 жыл бұрын
Dissolve the chloride. Use enough NaOH to ppt all of the zinc as the hyroxide. Wash precipitate and dissolve it in more NaOH. You then have your sodium zincate starting material.
@szymongolac7853
@szymongolac7853 2 жыл бұрын
Yes you can, but it will cause production of toxic Cl2 gas instead of O2 so it's a bit more dangerous
@HIB1968
@HIB1968 2 жыл бұрын
Hi, when i have drop my PGM’s with zinc can i recover the zinc I’ve used this way? thanks
@andrewhess4282
@andrewhess4282 7 жыл бұрын
Now how can I melt the zinc powder back down into solid zinc? I happened to come into possession of a large quantity of zinc powder, and every time I try to melt it into bulk zinc, it just burns. I don't have the wherewithal to put it under inert gas. Ideas?
@stephenjacks8196
@stephenjacks8196 4 жыл бұрын
FYI industrially zinc is plated using alkaline cyanide bath and also alkaline pyrophosphate solution. Rem electromotive force series is different in alkaline vs acid e.g. hydrogen is 0.0 volts in acid and -0.8 volts in alkali. Also the area around the negative electrode attracts zinc positive ions not negative zincate ions; need agitation.
@Valkyre_001
@Valkyre_001 8 жыл бұрын
Could you explain why this process gives a spongy zinc layer and an acid process does not?
@parcydwr
@parcydwr Ай бұрын
@NurdRage I am wanting to purify some zinc for our periodic table. My source material is some rather nasty corroded zinc from dead zinc-chloride batteries. I have saved the manganese dioxide / electrolyte paste and carbon electrodes.i am just wondering if a lye in water solution will dissolve the zinc and zinc oxides, maybe chlorides or other corrosion products? Would the electrolysis process then leave contaminates in solution and maybe also form an anode sludge of less soluble material? I am not a chemist, just trying to work things out to keep my two son's interested in doing these experiments.
@GrantFrankBurton
@GrantFrankBurton Жыл бұрын
Can you make a video on how to Recycle zinc sulfate.... how to separate the zinc from sulfuric acid and not destroy the acid other then distillation. I tried with Electrolysis, the moment I cut the power the zinc goes back into solution. even diluting the solution, I can't get the zinc out fast enough. Or maybe it's just not possible?
@graywolf2600
@graywolf2600 8 жыл бұрын
Any reason why this process creates a sponge versus a plate like the acid process?
@seffymidtatawa9323
@seffymidtatawa9323 4 жыл бұрын
can you show us how to make brass solution or how to make activator?
@FLYINGDUTCH2000
@FLYINGDUTCH2000 Жыл бұрын
Is it also possible to use ather metals like RVS for the anode and kathode of something?
@AJ-sj3cj
@AJ-sj3cj 3 жыл бұрын
Is there any substance works in the place of sodium acetate to form zinc powder
@Koroistro
@Koroistro 8 жыл бұрын
How energy hungry of a process is this? How many joules of energy for a gram of Zinc yeld? I know i could check the Delta G of the reaction but how energy efficient of a process is this?
@ThePatos1
@ThePatos1 5 жыл бұрын
how to activate zinc to use it as a reducing agent with acetic acid?
@Hobypyrocom
@Hobypyrocom 8 жыл бұрын
what mesh size of zinc particles will this produce?
@TextuallyActive122
@TextuallyActive122 8 жыл бұрын
Hey NurdRage, will you be doing your Q&A's anytime soon, or is that series dead?
@dalitas
@dalitas 8 жыл бұрын
I'll be honest... we... I need more videos! :)
@Taha-hv6yj
@Taha-hv6yj 4 жыл бұрын
Is it pure zinc? Cuz I'll react it with methyl iodide to make methylzinc
@krisztianszirtes5414
@krisztianszirtes5414 8 жыл бұрын
Don't forget that you can purify zinc in this method very efficiently with little to no waste products
@Peppersfuckingrule
@Peppersfuckingrule 8 жыл бұрын
What are you going to use the Zn for?
@benearhart1224
@benearhart1224 2 жыл бұрын
If you take the zinc out, scrape it off, and wash it immediately 3 times with dH20, then twice with acetone, you have yourself activated zinc. Be sure to dry it under an inert atmosphere because it is pyrophoric.
@sanjeevkumargill919
@sanjeevkumargill919 Жыл бұрын
Sir how much walts and amps have to be given
@07Timmers
@07Timmers 6 жыл бұрын
Can u use potassium hydroxide inside of sodium hydroxide?
@jaydaksrules5316
@jaydaksrules5316 8 жыл бұрын
Can this be done with tin oxide? to make tin powder.
@rajnipandya3302
@rajnipandya3302 4 жыл бұрын
Can we separate zinc from copper sulphate electrolyte by this method??
@carlmartel8510
@carlmartel8510 6 жыл бұрын
Can another metal be used at the anode?
@il_vero_saspacifico6141
@il_vero_saspacifico6141 3 жыл бұрын
It work It i put a block of zinc and not zinc oxide?
@yogeshbadgujar5398
@yogeshbadgujar5398 4 жыл бұрын
Hi sir I want to extract zinc from zinc ash please do a video on that.
@user-sx5si1sq3j
@user-sx5si1sq3j 7 ай бұрын
Great video: Do ​​I need to wash with hot water? A second question: Can we use it for precipitation, but rather aqua regia?
@HeisenbergADHDScienceAndMore
@HeisenbergADHDScienceAndMore 5 жыл бұрын
It would be good to reduce iodoalkanes. Like reducing iodocyclohexane to cyclohexane using zinc powder and acetic acid.
@Tokimime31
@Tokimime31 8 жыл бұрын
I know that a person can get aluminum chloride by dissolving aluminum in hydrochloric acid, is it possible to reverse this to get aluminum from aluminum chloride? If it is possible how is it done?
@akhilthechemist
@akhilthechemist 7 жыл бұрын
you must use a wire at cathode that would prevent zinc plating and give you crystals of zinc.
@Prchemist06
@Prchemist06 3 жыл бұрын
Hey! I want to know your confirmation about the method that this method will work with aluminium oxide or foil ...
@JoakimfromAnka
@JoakimfromAnka 2 жыл бұрын
Can you remove zinc plating by electrolysis?
@ThePeterDislikeShow
@ThePeterDislikeShow Жыл бұрын
Can you show how to anodize zinc?
@muhammadbakr2783
@muhammadbakr2783 3 жыл бұрын
Can I use carbon instead of nickel?
@johnlaurits381
@johnlaurits381 2 жыл бұрын
Would this work with sodium carbonate rather than sodium hydroxide?
@alrehmatshirani8831
@alrehmatshirani8831 3 жыл бұрын
Simple shape where zink use...wich parts machinary have...please i want
@trollmcclure1884
@trollmcclure1884 Жыл бұрын
but will it clean the zinc from lead, cadmium etc? I've read that ammonium carbonate can do it somehow
@laurdy
@laurdy 8 жыл бұрын
can you show us how to make tin powder?
@crybabies2600
@crybabies2600 4 жыл бұрын
what is that metal or bullet something at the first?
@sciencestararvinsinghk
@sciencestararvinsinghk 7 жыл бұрын
can aluminum b done like this
@TheMono25
@TheMono25 3 жыл бұрын
Will sodium hydrogen sulfate work instead
@WindowsTutorial772
@WindowsTutorial772 3 ай бұрын
for aluminum, same process can be done with sodium aluminate ??
@shrikesavadithya6683
@shrikesavadithya6683 8 жыл бұрын
would there be any reaction with the copper circuit board and if yes then what would be produced ?
@gazzarrr666
@gazzarrr666 3 жыл бұрын
Not as the cathode, here. The fact that you are reducing zinc ions to metal, here, means that the cathode is kept at an electrical potential that ensures that it remains as a metal.
@DrAyoub-ln4ly
@DrAyoub-ln4ly 2 жыл бұрын
Can I use this process to obtain titanium from titanium oxide?
@kamilhultaj5006
@kamilhultaj5006 8 жыл бұрын
Actually, I have no single idea about all this but I find this enjoyable to watch since very long time. :)
@user-vg8cv6nx1k
@user-vg8cv6nx1k Ай бұрын
A question, please. Is the zinc oxide I made now toxic or non-toxic.?
@user-ix5gf4vm9t
@user-ix5gf4vm9t 9 ай бұрын
مرحبا صديقي هل يصلح الزنك هذه الترسيب الذهب من الملكي
@nivmoshe5536
@nivmoshe5536 8 жыл бұрын
NurdRage I have a question why you used zinc oxide to be dissolved in the sodium hydroxide solution if sodium hydroxide reacts with zinc at the same way?
@outofthebox5972
@outofthebox5972 6 жыл бұрын
Niv Moshe Maybe i can help you . Yes sodium hydroxide can react with zinc but if the process is working that doesn't happen cz at the same time you produce zinc metal so when finished the process you must to filter off the solution instantly. To protect your powder .and dry it with acetone or ethanol. And sry for bad english .
@vornamenachname6300
@vornamenachname6300 6 жыл бұрын
well, the point was to make the zink, so ...
@dice6918
@dice6918 Жыл бұрын
❤ thank you
@MuzikBike
@MuzikBike 8 жыл бұрын
Are you ever going to make any more chemical resistance videos? I would quite like to see palladium (which apparently dissolves in nitric acid alone, unlike platinum).
@Berghiker
@Berghiker Жыл бұрын
Can you show how to make ANILINE DYE? (PURPLE MAUVE) color.
@user-sg2yt6nc1z
@user-sg2yt6nc1z 4 жыл бұрын
Can you make aluminum powder by electrolysis??
@hwangmic
@hwangmic 7 жыл бұрын
How do you control the voltage? I want to do something like this for an IB chemistry investigation. I plan on exploring how different voltages affect the rate of reaction using the method you used in this video.
@recessiv3
@recessiv3 7 жыл бұрын
Michael Hwang Variable power supply. About $100 at a local electronics store (cheap kind anyway) Additionally you can get a 120 volt transformer with about 5 amps and just add resistors... Wouldn't recommend it though
@benearhart1224
@benearhart1224 2 жыл бұрын
you need a current supply ideally.
@VerbenaIDK
@VerbenaIDK 2 жыл бұрын
a benchtop variable power supply should do it
@mobalottt
@mobalottt 7 жыл бұрын
What voltage and how much current did you use? Did you use AC or DC?
@stephenjacks8196
@stephenjacks8196 4 жыл бұрын
He said positive electrode and negative electrode. There is plus and minus on a battery not an AC cord.
@aminassadi5104
@aminassadi5104 2 жыл бұрын
it is so useful
@aaronward6092
@aaronward6092 3 жыл бұрын
Your solution gets clear so quick. Lol
@mattibboss
@mattibboss 8 жыл бұрын
can KOH be used?
@thecrudelab3204
@thecrudelab3204 5 жыл бұрын
can you do this with aluminium?
@mihajlopetkovic2003
@mihajlopetkovic2003 5 жыл бұрын
Can you use zinc anode in concentrated sodium hydroxide solution so that you leach zinc from anode and deposit it as a powder on cathode?
@neutronpcxt372
@neutronpcxt372 5 жыл бұрын
Yes.
@DulgenukChannel
@DulgenukChannel Жыл бұрын
How to powdering tin?
@katodisadeputki5695
@katodisadeputki5695 3 жыл бұрын
Does the nickel electrode wear?
@mohsenium
@mohsenium 2 жыл бұрын
Can we do this with aluminium also ?
@dave6733
@dave6733 7 жыл бұрын
@NurdRage Can this work with Magnesium Chloride or Magnesium Hydroxide?
@stephenjacks8196
@stephenjacks8196 4 жыл бұрын
Magnesium doesn't dissolve in Sodium Hydroxide because it doesn't form anything like "zincate". Reactive metals don't electoplate well from water solutions.
@bedouintrader
@bedouintrader 5 күн бұрын
what was the color of zinc oxide ??? I didn't see it well
@Mylitla
@Mylitla 8 жыл бұрын
It would be interesting to see the electroless zinc plating of aluminum using the zincate process. You're more than half way there.
@mr.0x373
@mr.0x373 2 жыл бұрын
Could this work with aluminum?
@FriendJamie
@FriendJamie 8 жыл бұрын
This is slightly terrifying... totally amazing
@akaruikage8576
@akaruikage8576 8 жыл бұрын
Very nice Video! But I have a question: Can you do the same procedure with aluminum oxide? Or do you need a different solvent?
@neutronpcxt372
@neutronpcxt372 5 жыл бұрын
No. Aluminium reacts with sodium hydroxide to form sodium aluminiate.
@MustafaAhmed-rr8wu
@MustafaAhmed-rr8wu 2 жыл бұрын
@@neutronpcxt372 mean we can do the aluminium powder with the same steps ? Or no
@lautaromorales2903
@lautaromorales2903 2 жыл бұрын
@@MustafaAhmed-rr8wu aluminum is highly reactive, so it can't be deposited in the cathode, and only hydrogen is going to be reduced
@lautaromorales2903
@lautaromorales2903 2 жыл бұрын
but this can be done with lead
@vabbe71
@vabbe71 2 жыл бұрын
Can I make nickel powder the same way?
@CFFNC
@CFFNC 8 жыл бұрын
I didn't think it was possible to reduce zinc metal out of water. Really glad you posted this, now I can finally use that giant bag of zinc oxide for something and won't have to grind down zinc for powder anymore.
@07Timmers
@07Timmers 6 жыл бұрын
What were the volts and amps you were using to make zinc?
@lakshminarayana6045
@lakshminarayana6045 3 жыл бұрын
I have the same question?
@sanjeevkumargill919
@sanjeevkumargill919 Жыл бұрын
Sir, I couldn't do it either. Do you know anything about Volts and amps please tell me ?
@KsatriaChannnel
@KsatriaChannnel 2 жыл бұрын
Voltase? Ampere?
@dorzsboss
@dorzsboss 6 жыл бұрын
what voltage did you apply?
@igrewold
@igrewold 6 жыл бұрын
1:20 Ain't sure but try 12V 1 Amp then like he said drop to %20 current( .2A = 200mA ) For electrolysis current is more important than voltage but since voltage is a path to current then it must be high(12v) See this, if you got a variable power supply like Gophert, it will read you how much voltage/amperage(current) is being consumed by electrolysis or use 2 cheap DMMs if you only got a 12v dc adapter/source. the one that reads voltage connects parallel to +/- wires and the one that reads amperage/current connected in series, meaning before the + or - electrode. www.harborfreight.com/7-function-digital-multimeter-92020.html (if you already got a DMM then that is good so just get another and if not you want one of the DMMs to be decent(not very) like Aneng 8008 for example)
@problems-hf8ts
@problems-hf8ts 8 жыл бұрын
Are you no longer answering patron questions? good!
@qb6025
@qb6025 3 жыл бұрын
I don't understand, why it aggregates, not plating 3:57
@piashghosh3759
@piashghosh3759 5 жыл бұрын
How can I contact you??
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