Agilent GC Troubleshooting and Maintenance: Liner, Septum, and O-Ring Replacement

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Agilent GC Troubleshooting and Maintenance: Liner, Septum, and O-Ring Replacement

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Күн бұрын

Regular maintenance of your GC Inlet will help you avoid chromatographic issues and increase lifetime. In this video, Herb Brooks, an Agilent Service Engineer, demonstrates how to replace your inlet liner, septum, and O-Ring on an Agilent 7890 GC.
The frequency of maintenance depends on the number of samples you run. To demonstrate, Herb Brooks takes you step by step on how to take apart your GC Inlet and replace the necessary parts. Proper maintenance and procedures are crucial in maintaining your GC lifetime and ensuring optimal performance. Herb also discusses contamination indicators and various signs that a part needs to be replaced.
For Replacement GC Liners, Septa, and O-Rings, please visit: www.agilent.co...
To view our Agilent Inlet Liners for GC, visit: www.agilent.co...
Unsure about which parts match your GC applications? Use our Part Selector Tool at: www.agilent.co...
#Agilent #GasChromatography #Troubleshooting

Пікірлер: 19

@kavyasreechintalapudi 3 жыл бұрын

Could you please elaborate on the process of tuning the system after changing the liner and septum, including the parameters that should be checked to make sure everything is set?

@geoffstewart6617 6 жыл бұрын

Way to go Herb!

@pharmasolutionpakistan7668 2 жыл бұрын

Good information

@oskardumanski8538 5 жыл бұрын

How should I clean the channel where the liner must be placed, if some particles are present?

@bygtyma05 5 жыл бұрын

I use a long cotton swab and dip it in hexane or solvent. Focus on cleaning near the top of the inlet where the purge and split vent trap are. If you have particles on the gold seal, it's best to remove the column and either change out the gold seal or clean it with hexane. Best of luck...p.s. Herb and Daron taught me everything i know

@user-uk3rw6xh4k 4 жыл бұрын

If you mean any particles are on the bottom of the inlet "tube" where the liner is placed, than just do the steps like in video of replacing the Gold Seal (without replacing, of course). It is pretty simple and requires two more steps than just replacing a column.

@aen8921 8 жыл бұрын

How would you purge with carrier gas while the injector and column are still 'cold'?

@capchemist 7 жыл бұрын

You can pressurize the inlet without needed to turn on any of the heating elements. This can be achieved from your instrument's front panel, or by adjusting the instrument parameters in your software.

@szamanisticrealistic2659 6 жыл бұрын

Is it necessary to vent the mass spectrometer to replace the inlet liner ?

@agilent 6 жыл бұрын

No, you don’t need to vent your mass spec to change your liner and septum. All you need to do is turn off the gas flow on your GC. As best practice make sure heated zones are cooled prior to the replacement.

@nsy1087 4 жыл бұрын

For gcfid, do I replace the liner before or after the flame ignite

@angelicahall3701 4 жыл бұрын

Perform a liner replacement (and any other accessory replacements) prior to flame ignition.

@lycaetano 5 жыл бұрын

How can I replace the liner in GC with headspace?

@oskardumanski8538 5 жыл бұрын

The same way as in the GC without HS: 1.) Disconnect the transfer line (in modern systems transfer line is connected perpendicular to the liner and you don't need to disconnect it). 2.) Remove the cap (in older systems it looks more like a sleeve than a cap). 3.) Replace liner with accordance to the movie.

@jesusa1885 6 жыл бұрын

How often should you do this?

@agilent 6 жыл бұрын

When to change the septum, liner ad O-ring depend on the analysis you are running how many injections are done a day, how clean the sample is, and what type of liner you are using. In January we did a Webinar on Healthy Habits of GC, through Separation Science. Here is a link. This should provide you with some good information. webinar.sepscience.com/habits-for-a-healthy-gc-insider-tips?hsCtaTracking=98fc9cbe-7a6d-429d-880f-01b5070d1e5f%7C2eb27d2d-ae36-4d74-b1f9-38302a368b7d