Attempting to make a ferrofluid

  Рет қаралды 4,659,428

NileRed

NileRed

5 жыл бұрын

In this video, I'll be attempting to make ferrofluid from the ferric chloride and ferrous sulfate that I made in a previous video. At first, I thought that this project would be really straightforward, but it turned out to be much more difficult than I thought.
I am going to be working more on this project, and I hope that soon I'll have an easy method to make it from relatively easy to get chemicals and supplies.
References:
• Coated nanoparticle photo source: goo.gl/CtTsxU
• Making Iron (II) sulfate: • Recreating one of the ...
• Making Iron (III) chloride: • Making Prussian Blue
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Nile talks about lab safety: • Chemistry is dangerous.
Music in credits (Walker by SORRYSINES): / walker

Пікірлер: 3 800
@SympackLaboratories
@SympackLaboratories 5 жыл бұрын
"Cheap things like printer toner"
@bruhhelp7396
@bruhhelp7396 5 жыл бұрын
Lol
@rat_lives_matter9136
@rat_lives_matter9136 4 жыл бұрын
Lol
@ALi-bm9io
@ALi-bm9io 4 жыл бұрын
Lol
@addvacx5214
@addvacx5214 4 жыл бұрын
Lol
@velvet1250
@velvet1250 4 жыл бұрын
lol
@vickyevan2279
@vickyevan2279 4 жыл бұрын
Me: *needs to sleep* My brain: NO watch the CHEMISTRY MAN
@robertrostron1550
@robertrostron1550 4 жыл бұрын
Its literally 2am here haha
@maximumaction1125
@maximumaction1125 4 жыл бұрын
Me at 4 in the morning
@triptomoon9870
@triptomoon9870 4 жыл бұрын
So you and your brain are different beings?
@equaius893
@equaius893 3 жыл бұрын
@@triptomoon9870 its called a joke
@aidan7458
@aidan7458 3 жыл бұрын
Chemistry man... He awaits...
@SeSaGaming
@SeSaGaming 2 жыл бұрын
Just wanted to say, the FerroFluid wrapping down the screw was one of the most relaxing things to watch.
@skelly175
@skelly175 Жыл бұрын
Damn, catalyst must have studied this video for years.
@MRafas-ie9zh
@MRafas-ie9zh Жыл бұрын
KZfaq algorithms are sure awesome
@John4Real
@John4Real Жыл бұрын
This video is sponsored by EA 😂
@cowenthusiast4046
@cowenthusiast4046 Жыл бұрын
@@John4Real 😭😭
@Josh-ig1ve
@Josh-ig1ve Жыл бұрын
Lmaooooo
@MythicTrippy
@MythicTrippy Жыл бұрын
Was the first thing I thought od
@bradleylim993
@bradleylim993 5 жыл бұрын
This venom trailer looks awesome
@jasonfalzarano7888
@jasonfalzarano7888 5 жыл бұрын
Holy fuck Wear a magnet suit and pour this on yourself Venomize that shit
@cameronmosesart
@cameronmosesart 5 жыл бұрын
Stop it lol
@ziro7120
@ziro7120 5 жыл бұрын
exactly what I thought of lmao
@cordialmanx2334
@cordialmanx2334 5 жыл бұрын
@@jasonfalzarano7888 yaaaas
@palamagoose144
@palamagoose144 5 жыл бұрын
I know, right!
@CarnivorousPlantsAndGardening
@CarnivorousPlantsAndGardening 4 жыл бұрын
2:47 pause gentely jiggle your screen and it will appear to move
@lemonytrash584
@lemonytrash584 4 жыл бұрын
Oh god that’s messing with my mind
@iamjae1999
@iamjae1999 4 жыл бұрын
How
@yerischerries3010
@yerischerries3010 4 жыл бұрын
DUDE NO
@bellaisbork8416
@bellaisbork8416 4 жыл бұрын
lol
@remus6846
@remus6846 4 жыл бұрын
Ah shit how did this happend
@zexyoo6654
@zexyoo6654 Жыл бұрын
“Pierce through the mundane”
@SmashTheAdam
@SmashTheAdam 2 жыл бұрын
This channel really opened my eyes to how fun chemistry can be, if only schools did these kind of experiments from time to time
@jackni7863
@jackni7863 Жыл бұрын
But there legally required to be boring
@TheVivi13
@TheVivi13 Ай бұрын
These can get dangerous really quickly, do you really trust highschoolers to do this lol. In Uni chem you get to do a lot of cool stuff though with some pretty high tech equipment.
@N.N-Dimethyltryptamine
@N.N-Dimethyltryptamine 5 жыл бұрын
I don't think enough people tell you how professional and high quality your content is
@lepassant478
@lepassant478 5 жыл бұрын
Nice name. Where's that come from ?
@brentvettel5343
@brentvettel5343 5 жыл бұрын
Yup
@Leo-sx9jz
@Leo-sx9jz 5 жыл бұрын
second that!
@NileRed
@NileRed 5 жыл бұрын
:)
@polymerasiecondens6857
@polymerasiecondens6857 5 жыл бұрын
@@NileRed you are also undetrated, you deserve waaay waay more but ye you got an extra sub from me😁 and nice video man💯🔥
@stickoutofthemud
@stickoutofthemud 5 жыл бұрын
"Unsuccessful" experiments are just as important as the other kind. They should also be published.
@drunkensailor997
@drunkensailor997 3 жыл бұрын
Nile blue???
@thineevee7345
@thineevee7345 3 жыл бұрын
Nileblue
@stickoutofthemud
@stickoutofthemud 3 жыл бұрын
@@J.PC.Designs The kind that unqualifiedly prove the hypothesis tested
@scottpwood
@scottpwood Жыл бұрын
Who else got this recommend to them after season 15 of apex?
@Wouldyouinsertnamehere
@Wouldyouinsertnamehere Жыл бұрын
Me
@catalyst6264
@catalyst6264 Жыл бұрын
So that’s where my missing canisters went
@splatz3736
@splatz3736 Жыл бұрын
I knew someone would comment something like this 😂
@memphisdepay6161
@memphisdepay6161 5 жыл бұрын
"H2O is water" is the smartest thing i can say in chemical
@DanIsDistant
@DanIsDistant 4 жыл бұрын
@aud_io Liquid Gas
@conquestv4024
@conquestv4024 4 жыл бұрын
Dihydrogen monoxide
@joroc
@joroc 4 жыл бұрын
Hey I also know H2SO4 and NaCl 👆
@twopeople254
@twopeople254 3 жыл бұрын
CO2
@ophew
@ophew 3 жыл бұрын
liquid ice
@GippyHappy
@GippyHappy 5 жыл бұрын
"I definitely added way too much kerosene" **Ten seconds later** "So I'm just slowly adding more kerosene" **0.2 seconds after** "I think I used too much kerosene"
@donovanstringer7411
@donovanstringer7411 5 жыл бұрын
kerosene
@CharlesBosse
@CharlesBosse 5 жыл бұрын
I think it would be interesting to see if you can figure out the commercial solvent. I bet they don't use kerosene and that might make a big difference.
@biteme9869
@biteme9869 4 жыл бұрын
Christopher Walkensen who kerosene’s
@mchagnon7
@mchagnon7 4 жыл бұрын
Sometimes science isn't an exact science...
@jonnyphenomenon
@jonnyphenomenon 4 жыл бұрын
@@CharlesBosse polyethylene glycol perhaps?
@je36youtube
@je36youtube Жыл бұрын
Catalyst definitely watched this video
@pranavsuresh5783
@pranavsuresh5783 Жыл бұрын
lmao
@rooba4277
@rooba4277 Жыл бұрын
Definitely
@afdhal4026
@afdhal4026 Жыл бұрын
OMG! THIS PERSON HAS LEAKED CATALYST SKILL 4 YEARS AGO! WHAT AN INSIDER
@bappo218
@bappo218 5 жыл бұрын
Lisa Simpson's hair is ferrofluid and her skull is a magnet edit: i dont remember making this comment and i hate it just as much as you do
@TheoParis
@TheoParis 5 жыл бұрын
LOL
@okfirstofall4432
@okfirstofall4432 5 жыл бұрын
oh no
@PapagenoDispo
@PapagenoDispo 5 жыл бұрын
get that idea away from me
@agreenunderripebanana8901
@agreenunderripebanana8901 5 жыл бұрын
R/cursed comments
@buurman2635
@buurman2635 5 жыл бұрын
stop that
@tedCain1
@tedCain1 5 жыл бұрын
If you're watching on mobile, pause the video at 2:39 and slightly jiggle your phone back and forth.
@brockbland6788
@brockbland6788 5 жыл бұрын
What the heck. That’s pretty cool, my dude
@matthewludivico1714
@matthewludivico1714 5 жыл бұрын
I thought I saw Ender man for a second.
@astrielmaahes1116
@astrielmaahes1116 5 жыл бұрын
Strange wonder why that happens
@dylanhouchin
@dylanhouchin 5 жыл бұрын
I have no idea how you found that 😂
@lepassant478
@lepassant478 5 жыл бұрын
I saw that too !! Is it the black contrast that provoke this effect ? That's a surprising thing.
@sharynkerr8378
@sharynkerr8378 Жыл бұрын
Pierce their hearts! And their feet -somebody who is from Peak Myths or something
@crosstail8656
@crosstail8656 Жыл бұрын
Catalyst saw this shit and started plotting💀
@xaostek
@xaostek 5 жыл бұрын
I think this is why I love your channel, you're willing to show everything, even your failures or mistakes. Most science channels only ever seem to show a perfect product, but you offer an insight into the problem solving process whenever something goes wrong, and explain your thought process when figuring out what went wrong, why, and how to fix it. The problem solving is just as much a part of science as the "cool stuff" is.
@jonathanodude6660
@jonathanodude6660 5 жыл бұрын
codys lab is also good
@akersmc
@akersmc 5 жыл бұрын
Applied Science too.
@saumitjin5526
@saumitjin5526 5 жыл бұрын
@@jonathanodude6660 Any other chem channels you follow rather than these two?
@therealbobmayo5065
@therealbobmayo5065 5 жыл бұрын
dear nitro, thx ms. angry anime lady.
@Eseeetacoy
@Eseeetacoy 5 жыл бұрын
And that there is exactly what a scientist is.
@scottwallace4428
@scottwallace4428 5 жыл бұрын
No amount of training can prepare you for using the right beaker size ❤️
@surki2080
@surki2080 5 жыл бұрын
Lol
@abyssstrider2547
@abyssstrider2547 5 жыл бұрын
That sounded wrong... was it meant to?
@inowake
@inowake Жыл бұрын
10:35 his gloves stuck at under the magnet xD
@Richard.Andersson
@Richard.Andersson 5 жыл бұрын
Some tips from someone who have made a lot of magnetite nanoparticles in the past. 1. How pure the iron salts are can have a big impact on nucleation and there for particle size. The time the solutions spend in air will affect oxidation and hydrate complex formation. I always used chloride of both Fe II and III, never tried sulphate 2. Temperature during precipitation is important, colder is usually better based on experience and transmission electron microscopy (TEM) analysis. 3. Do not dry the particles fully, try and make solvent exchange, this will prevent aggregation. For example: water - acetone - toluene - kerosene (perhaps there are better routes, I have not done this myself, also I am not sure what is most compatible with kerosene) 4. Ultra-sonic treatment is often mandatory for good dispersion. Good luck :)
@MrNybios
@MrNybios 5 жыл бұрын
I made the experience, that Fe-NP from a hot wall reactor a much easier to handle and redisperse. You could put these particles in some sunflower oil and get a fairly stable ferrofluid. Chemical synthesized Fe-NP are very hard to handle, mostly because of the ligands. Not a fan of this method to produce NP, espacially for a purpose like this.
@NileRed
@NileRed 5 жыл бұрын
My next attempt will use an ultrasonic bath and an overhead mixer missing it super quickly. I will also use a nitrogen atmosphere to limit the oxidation. Why is it that some people tell me that heat is absolutely necessary but others say that cold is usually better?
@Shodkev
@Shodkev 5 жыл бұрын
@@NileRed Im not an expert but on all the synthesis on nanoparticles that ive done most papers call for extremely dilute solutions in order to prevent aggregation, maybe if you drop down the concentration aggregation shouldn't be that much of an issue
@tobiasseitz4914
@tobiasseitz4914 5 жыл бұрын
This depends on the synthesis you're pulling off. Using a hot solution to inject the reuducing agent, you'll get a monodisperse phase with the NPs being pretty homogenous in size (called the Hot-Injection-Method). You'll need a dillute solution and relatively strong coulomb or sterical inhibition. Using cold solutions can lead to higher concentrated suspensions, I'd guess, and can get along with less good inhibiton. Your particle growth and size are going to be more heterogeneous, though. I did it both ways once and I have to say that the temperature can get quite high if your inhibitor is good. Usually, sterical inhibition is good for long-term storage and more reliable, but Citrate was able to stabilise our Au-NP solution at temperatures around 80 °C by coulomb repulsion.
@FishbedMyBeloved
@FishbedMyBeloved 4 жыл бұрын
Me, who knows absolutely nothing and just watching this thread progress
@SafetyLucas
@SafetyLucas 5 жыл бұрын
Try evaporating the kerosene away until it spikes. Also, the brown color may not be from contamination but rather the particle size. Nano particles have different optical properties from macro scale particles.
@greenthizzle4
@greenthizzle4 5 жыл бұрын
Safety Lucas true, like nano gold is red
@leocurious9919
@leocurious9919 5 жыл бұрын
Pretty sure its from the iron, its such a charachteristic color. Not to mention that its a mix of 2 colors, so it would have to be two very specific sizes of particles. Highly unlikely.
@xuanbachlai5371
@xuanbachlai5371 5 жыл бұрын
nano gold particles can easily reach small sizes, that's why they are prime examples for varied colors. Iron oxides? Pretty tough.
@greenthizzle4
@greenthizzle4 5 жыл бұрын
Xuan Bach Lai you can make nano ferrite down below 5nm
@greenthizzle4
@greenthizzle4 5 жыл бұрын
Xuan Bach Lai it takes other kinds of processes then the standard process he's using though.. But it possible
@chaos8271
@chaos8271 Жыл бұрын
this definitely only showed up on my feed because the new apex character
@GDaddyTx
@GDaddyTx 9 ай бұрын
This is so interesting, can’t wait to see further progress
@boy6821
@boy6821 5 жыл бұрын
This was by far the best episode of Full Metal Alchemist
@gabor3849
@gabor3849 3 жыл бұрын
XD
@qqwee9014
@qqwee9014 3 жыл бұрын
@Chairman of Toes Don't throw your stupidity here.
@aliveandunwell430
@aliveandunwell430 3 жыл бұрын
Sarcastic Studios r/murderedbywords
@movedchannels1105
@movedchannels1105 3 жыл бұрын
This is alphonse giving us a tutorial
@Stankboi
@Stankboi 3 жыл бұрын
Full metal alchemist when the alchemists discover full metal idk i didnt watch the show
@askhowiknow5527
@askhowiknow5527 5 жыл бұрын
I need to get my ears checked. You said “hard drives and speakers” and I heard “hard drugs and sneakers” and was intrigued
@zualapips1638
@zualapips1638 5 жыл бұрын
Could just be your brain.
@U014B
@U014B 5 жыл бұрын
Must be all the hard drives you've been taking.
@KhushiSharma-ci2kf
@KhushiSharma-ci2kf 5 жыл бұрын
I heard hard drugs or speakers
@yawn6986
@yawn6986 5 жыл бұрын
I heard drive ways and speakers for some reason. XD Brains are weird
@Legominder
@Legominder 5 жыл бұрын
Or you need to check your speakers.
@magnify4720
@magnify4720 2 жыл бұрын
i don't know anything about chemistry, and i never understand what u do. but it's always so incredibly interesting just seeing everything react with each other and you doing stuff and trying to explain it to my tiny brain. well done dude.
@steadfast1448
@steadfast1448 Жыл бұрын
Same thing m8
@jadedrip6208
@jadedrip6208 2 жыл бұрын
NileRed: "It looks like magic" Me: "I think that is Venom"
@aumbhatt5339
@aumbhatt5339 2 жыл бұрын
Even I thought it looked like venom
@ZJArt
@ZJArt 5 жыл бұрын
Clicked because I thought it was a 3D render (tutorial), stayed for science
@daneilgame123
@daneilgame123 2 жыл бұрын
**insert creative reply**
@thelocalnecromancer1224
@thelocalnecromancer1224 2 жыл бұрын
@@daneilgame123 *insert creative reply to your creative reply*
@eyemoisturizer
@eyemoisturizer 2 жыл бұрын
@@thelocalnecromancer1224 **insert really uncreative reply to your creative reply to a creative reply**
@vergil2
@vergil2 2 жыл бұрын
@@eyemoisturizer *insert really creative reply to your uncreative reply to a creative reply to a creative reply*
@Withern679
@Withern679 2 жыл бұрын
@@vergil2 *insert a mildly creative response to your really creative reply to their uncreative reply to a creative reply to a creative reply*
@jansenart0
@jansenart0 5 жыл бұрын
ALWAYS PUBLISH YOUR FAILURES! Very happy see this! 😊
@PhillipAmthor
@PhillipAmthor 5 жыл бұрын
Im glad my parents published me now, thanks!
@schnoig_
@schnoig_ 5 жыл бұрын
Ichbims Derepep this is such a bruh moment
@foxoboxo1233
@foxoboxo1233 Жыл бұрын
This showed up in my recommended feed right after I watched the Apex Season 15 trailer
@jonathanjoestar3173
@jonathanjoestar3173 3 жыл бұрын
0:48 the forbidden blackberry fruit snack
@joshualeefyi
@joshualeefyi 5 жыл бұрын
I don't mean to sound like a know-it-all because I have no clue but do you think the stir bar you have may have had an adverse reaction as far as the magnetic movement
@Kineth1
@Kineth1 5 жыл бұрын
My thoughts exactly: "You're trying to make the magnetite particles as small as possible, but you're putting a magnet into them and pulling them together when you're trying to coat them"
@urdnal
@urdnal 5 жыл бұрын
Yeah same as what I thought (though I barely know more about chemistry than your average layman). I kept waiting for him to mention something about it but...
@anlm1
@anlm1 5 жыл бұрын
I'd have to disagree. I made a good quality sample that formed spikes while using the stir bar. The ratio of concentration of Fe2+ ions to Fe3+ ions is an absolutely critical component to making proper particles and is documented in literature. The ratio of oleic acid used also plays a noticeable role in sample quality if I remember correctly. The only issue I had with the sample was that i left it overnight in the ammonia solution it was made in and returned to brown gunk like that in the morning. So the only sample I have left was from my first attempt which also just made a small bulge like in the video, but stayed in suspension it was of lower wuality because I did not get the ratio of Fe2+ to Fe3+ ions down as close to perfect as it needed to be, it is very sensitive to deviation from that ratio.
@anlm1
@anlm1 5 жыл бұрын
Also as a side note, I also recall having that hydrophobic clumping thing occur. I don't remember how exactly was resolved but i think it was by dripping a bit of HCl in to lower the ph again. And mrhomescientist had a great video on how to make ferrofluid, which Is pretty much the procedure I used just slightly changed up some things to have higher precision. kzfaq.info/get/bejne/gtKBqpyVy8vccoU.html
@artej11
@artej11 5 жыл бұрын
Good thing about it though is that it will discriminate by mostly affecting larger particles with bigger total magnetic moment(larger volume since it looks like single domain will be prelevant). For a given magnetic moment there should be maximal particle size stable on its own in solution. IMO stuff stuck to stirbar can be discarded outright. I might post later if I get not lazy enough to calculate limits imposed by the magnets. If somebody wants to do it separately it is just using Boltmans law to calculate when equilibrium concentration on magnet surface (proportional to e^(-m H)/kT) is enough so that distance between particles is enough so that energy of dipole interaction between particles is around kT.
@CinnamonToastKing
@CinnamonToastKing 5 жыл бұрын
Actually admits early on and confirms this is an attempt and failed as to prevent any possible clickbait. You my friend are better then a large majority of KZfaqrs , also very entertaining!
@sleepjamal
@sleepjamal Жыл бұрын
Catalyst's favorite KZfaq video
@gabszawa
@gabszawa Жыл бұрын
daamn apex science moment
@GamersBar
@GamersBar 5 жыл бұрын
Never worry about showing failed attempts , tbh its more interesting and people would prob learn more
@NileRed
@NileRed 5 жыл бұрын
I also like showing the failures. They are usually a better lesson than the sucesses
@Wishingweezy
@Wishingweezy 4 жыл бұрын
@@NileRed nile weezy can u please do a video on making white phosphorous from red one
@Sonnydaycreations
@Sonnydaycreations 5 жыл бұрын
2:39 if you’re watching on your phone shake it lightly while staring at the powder
@reaperroseyt203
@reaperroseyt203 3 жыл бұрын
I saw this on my own and made a comment damn its cool
@poulosegeorge5457
@poulosegeorge5457 3 жыл бұрын
Ya man its right its pretty cool
@adore_reh
@adore_reh 3 жыл бұрын
That's cool😂👍🏽
@snipermonke5722
@snipermonke5722 2 жыл бұрын
Oh no my eyes their broken
@vedanlkektokekto6872
@vedanlkektokekto6872 Жыл бұрын
It also work when light watch night when not can see border and shake
@williamcagle7359
@williamcagle7359 2 жыл бұрын
It's awesome to see someone that actually trys
@larrybanks1483
@larrybanks1483 9 ай бұрын
Never gets old watching.
@BlueMCer
@BlueMCer 5 жыл бұрын
In high school I was really enthusiastic for Chemistry and pretty good at it too, a chemistry degree was my second choice. Watching your videos (not this one in particular) makes me recall why I was so enthusiastic and makes me want to do some chemistry again! :D
@jameelakk4149
@jameelakk4149 2 жыл бұрын
This comment made me happy for some reason.
@vergil2
@vergil2 2 жыл бұрын
This comment made me happy for some reason.
@vodkaboi4974
@vodkaboi4974 2 жыл бұрын
And what was your first choice ?
@9393jack
@9393jack 5 жыл бұрын
Nothing is better than a nice calm educative NileRed video at the end of the day
@aayushpaswan2941
@aayushpaswan2941 2 жыл бұрын
dopplers effect :- kzfaq.info/get/bejne/pLt5qKeku8venYE.html
@aayushpaswan2941
@aayushpaswan2941 2 жыл бұрын
dopplers effect :- kzfaq.info/get/bejne/pLt5qKeku8venYE.html
@dAni-ik1hv
@dAni-ik1hv 2 жыл бұрын
i listen to this dude and learn nothing but still enjoy it
@AL3X_69
@AL3X_69 Жыл бұрын
Ferrofluid: *exists* apex legends fans: catalyst
@somedude6833
@somedude6833 5 жыл бұрын
9:10 "Mr Stark i don't feel so good" times 100.
@missandy6527
@missandy6527 5 жыл бұрын
C mamut
@rat_lives_matter9136
@rat_lives_matter9136 4 жыл бұрын
Lol
@thineevee7345
@thineevee7345 3 жыл бұрын
Bruh I just got an ad :'(
@pauldickinson3961
@pauldickinson3961 3 жыл бұрын
100? The ad said 3000.
@ralphggamer778
@ralphggamer778 2 жыл бұрын
THE BLIPP
@blubb7711
@blubb7711 5 жыл бұрын
Hey, have you got my mail about this topic? -Add the iron solution (1.5M) to the ammonia, not the otherway around. The fallout should be blacker than yours. -don´t pull out the magnetite straight from the solution, it will clump up. Instead add your oleic acid, about 5ml per 30ml of iron solution and bring it up to 80°C. ( I use Fe(II)Cl und Fe(III)Cl, I never tried the sulfates.) I never got the magnetite crash out by itself, I usally disolve it in petroleum, seperate the phases and crash it out with acetone from the petroleum. Everything left in the water is thrown away, because these particles aren´t coated enough. After crashing them out with acetone and a magnet, I redisolve it in petroleum (or n-Hexan/ n-Heptane). After this you should see small spiked when placing a magnet benath it. Then you have to supersatured the solution by letting it sit in the sun, or a another soft heat source for 2 weeks. It will thicken up and some bigger particles will fall out of solution. 13:15 this guy actualy gave me the idea of using acetone. 17:19 the color of your particles is way of, check the quality of your starting reagents. 19:10 spiking only acours when the solution is highly concentrated.
@bernardo00124719
@bernardo00124719 5 жыл бұрын
nice
@nilaksh007
@nilaksh007 5 жыл бұрын
Really helpful
@kokorec5598
@kokorec5598 4 жыл бұрын
you should've start by saying ''smart person to smart person''
@anthonypeterson777
@anthonypeterson777 3 жыл бұрын
6:16 ‘forbidden coffee’ 😁
@gregfairburn2253
@gregfairburn2253 3 жыл бұрын
Nevermind pausing it. Just screenshot it. Truly mindboggling. What type of wizardry is this.?? NileRed you sir are dabbling in black magic.
@not_my_name5200
@not_my_name5200 5 жыл бұрын
1:28 "Cheap things like printer toner" made me laugh uncontrollably
@zoe-xx
@zoe-xx 2 жыл бұрын
Innit
@verdatum
@verdatum 5 жыл бұрын
From what I know about pigment science, your problem isn't "filtering" particles that are too big or not coated. Your problem in the criticality of milling your particles. Milling after mixing with oleic acid should both reduce particle size, and force the lipids to bind. Unfortunately, milling is also a seriously tedious process, and often introduces contaminants in the form of grit. But it is a noble task, and I think it may be worth that effort.
@moronicpest
@moronicpest 5 жыл бұрын
Yes. It sounds to me like the problem is proper dispersion and wetting of the solid particles. In the paint industry sand mills are often used, where the pigment particles get coated and ground with a proper wetting agent and/or resin, and then stay properly dispersed once thinned with other paint ingredients. After 10 to 15 minutes of milling with external water cooling, the sand is filtered out through a strong metal mesh screen while the mill is still turning, forcing the thick liquid through mesh. Not sure if a small amount of fine sand particles would prevent the iron particles from working properly as a ferrofluid though, it would just have to be tested. I don't think Nile would have easy access to this type of a setup though.
@GLITCH_-.-
@GLITCH_-.- 5 жыл бұрын
It sounds like that would destroy the coating. I mean it will certainly "break most particles in half", wouldn't it?
@moronicpest
@moronicpest 5 жыл бұрын
What it does is divide agglomerates of particles and surrounds each particle with some of the dispersant so the particles won't re-agglomerate and will stay dispersed in the fluid medium, which is the end-game desired. They are using oleic acid in this case, but other longer chain molecules could possibly be used and might even do a better job at dispersing. A certain amount of trial and error is often involved in finding the best dispersant for each type of solid particles you are trying to disperse.
@GLITCH_-.-
@GLITCH_-.- 5 жыл бұрын
@@moronicpest I imagined them being crystals. Ok :)
@aayushpaswan2941
@aayushpaswan2941 2 жыл бұрын
dopplers effect :- kzfaq.info/get/bejne/pLt5qKeku8venYE.html
@RubbyBTD
@RubbyBTD Жыл бұрын
This getting recommended again cause of Apex
@maryljson
@maryljson Жыл бұрын
Foiler fluid made me chill its so satisfying
@scruzandrew
@scruzandrew 5 жыл бұрын
Some things to consider: 1) In general nanomaterial synthesis, the surfactants are included in the reaction mixture during nanoparticle formation to stabilize the particles and restrict their growth. 2) For a ferrofluid to work you must produce superparamagnetic magnetite, which means the particles size should be on the order of 20 nm or less. 3) Though aqueous precipitation methods are common, you have less control over particle size. One way around this is to first form the organometallic complexes (Fe-oleates) and then proceed with the nanoparticle formation (though these are typically high temperature reactions), the particles will form while maintaining a complete oleate coverage on each particle and remain very small and highly crystalline which will improve the yield of superparamagnetic particles with a high magnetic susceptibility. 3) The color changes from black-brown-black during your purifications are (imo) most likely due to aggregation in the various solvents as the overall diameter of the aggregate changes so will the color and the rate of separation. Note that oxidation of the magnetite over time (especially in aqueous solvents) will lighten the material to a lighter brown over time and iron species at the surface will dissolve into solution which can eventually desorb your surfactant and destabilize the material. 4) You may wish to degass your aqueous reaction mixture to reduce oxidation. As others pointed out: 1) Sonication! it's something I could not live without when it comes to nanochemistry (can get a jewelry cleaner pretty cheap and should work just fine for most uses). 2) >98% purity iron salt hydrates are pretty cheap, try and get some. 3) NaOH can be used if you don't need the ammonia-oleate reaction. 4) In many cases, the faster nucleation takes place, the smaller and more uniform your particles should be. 5) Magnetic stir bars will not adversely affect your reaction as long as you particles remain small and stable enough (as you correctly state they will not separate because their solubility is greater than the magnetic attraction force), however, if your reaction mixture is too large, mixing can become a problem and stir bars typically will not compete with a good overhead stirrer. Anyways, great to see you covering some nanochemistry and a room temp benchtop method as well! Good luck!
@johnrichard976
@johnrichard976 5 жыл бұрын
Youre video got featured on a Daily dose of Internet Video! I'm so happy.
@gamingoose5033
@gamingoose5033 3 жыл бұрын
What one?
@ownitervi241
@ownitervi241 2 жыл бұрын
Which one?
@boggn
@boggn 2 жыл бұрын
Who one?
@jansendonelmanalese3316
@jansendonelmanalese3316 2 жыл бұрын
Why one?
@r.ndomperson
@r.ndomperson 2 жыл бұрын
How one?
@jessica11773224
@jessica11773224 9 ай бұрын
I find it sooo soothing to watch 😁🥰
@thericehatwok2375
@thericehatwok2375 Жыл бұрын
*Catalyst has entered the chat*
@libertyprime69
@libertyprime69 5 жыл бұрын
Well, now we know why it's so expensive...
@animalanimalanimal1622
@animalanimalanimal1622 5 жыл бұрын
Can’t wait for the next batch!!
@tupacshakur8552
@tupacshakur8552 Жыл бұрын
I guess the new Apex Legends season must’ve brought me here
@heitorsant1759
@heitorsant1759 Жыл бұрын
What a gr8 video!!!!!! I loved the where he said: "IT IS NILEREDDING TIME!!!!!"
@Skeb90
@Skeb90 4 жыл бұрын
Hey NileRed, love your Videos - you'll probably not read this because I'm late to the party but: If you're worried that the Magnetite oxidizes too much while stirring, you could try to do that process under a non-reactive heavy gas. You'll need to prevent excessive spillage of the gas but you'd rule out oxidation.
@Joshishoss
@Joshishoss 5 жыл бұрын
somehow i always make my way here when im baked.
@thelocalnecromancer1224
@thelocalnecromancer1224 2 жыл бұрын
Baked?
@MarvelousButter
@MarvelousButter 2 жыл бұрын
@@thelocalnecromancer1224 it means high
@thelocalnecromancer1224
@thelocalnecromancer1224 2 жыл бұрын
@@MarvelousButter no
@MarvelousButter
@MarvelousButter 2 жыл бұрын
@@thelocalnecromancer1224 wdym no
@thelocalnecromancer1224
@thelocalnecromancer1224 2 жыл бұрын
@@MarvelousButter no, no
@alexhicks9535
@alexhicks9535 3 жыл бұрын
I'd love to see a part 2 if it's still a project your working on
@Lemu_with_a_shirt
@Lemu_with_a_shirt 2 жыл бұрын
He already made a follow up to this, a few videos later.
@RedTail94
@RedTail94 2 жыл бұрын
This reminds me of the movie Splinter with how it moves and looks, it's pretty neat!
@D0M3e
@D0M3e 5 жыл бұрын
Hallo Nile. The reason for your Brown colour is that you have a lot of rust in it. I had the same problem at university. After you produce your nanopartikel, you need to was them with water and enthanol. Then dry them and do the step with oil acid at the next Day. Then you can take the particels and suspend them in Olive oil. If you want, you can take a soap Solution and put the suspension inside. Then you can get a very nice ferrofluid :)
@UnbipentiumM
@UnbipentiumM 5 жыл бұрын
English isn't your first language, is it?
@mannyheffley9551
@mannyheffley9551 5 жыл бұрын
@@UnbipentiumM he's most probably Indian or German
@nilaksh007
@nilaksh007 5 жыл бұрын
@@mannyheffley9551 surely not indian but how does it matter ?
@blue.1
@blue.1 5 жыл бұрын
@@nilaksh007 his grammar is why.
@mycelia_ow
@mycelia_ow 5 жыл бұрын
@@blue.1, I'm a native english speaker and despite his misspelling and grammar, I could still understand what he was saying. Why's it a problem?
@TheFlipside
@TheFlipside 5 жыл бұрын
Hey I know this isn't the type of thing you normally do, but can you look into doing a video on alkalides? They're salts where the anion is a negatively charged alkali metal. I first heard of them a few days ago and looking at the procedure for their synthesis, it seems really interesting, though fairly expensive. Plus I haven't found any videos on them anywhere on KZfaq, so it could be a neat thing to show off
@stefangadshijew1682
@stefangadshijew1682 5 жыл бұрын
Can you share the synthesis? I'd bet it needs an inert atmosphere, negatively charged alkali metals sounds like it just wants to be with water. I also want to see this. :D
@Unterhosegotti
@Unterhosegotti 5 жыл бұрын
@@stefangadshijew1682 na- in water??!
@TheLouisph
@TheLouisph 5 жыл бұрын
I looked it up, its not stable in normal atmosphere and nile does not seem to have the proper equipment to deal with this kind of synthesis (Schlenk line or glove box)
@ouroya
@ouroya 5 жыл бұрын
this seems very unlikely, but electrides are interesting as well and more viable
@TheFlipside
@TheFlipside 5 жыл бұрын
@@ouroya I honestly thought electrides would be harder to make. Also yeah he probably doesn't have what he needs to do it but it's still an interesting thing to think about, so I figured it was worth bringing up
@phybrix1459
@phybrix1459 2 жыл бұрын
Man, you would be the best science teacher ever.
@dogeinchernobyl7257
@dogeinchernobyl7257 2 жыл бұрын
I love how he always sounds confused or unknowingly
@anthonycaminiti8734
@anthonycaminiti8734 5 жыл бұрын
Nile red and elemental maker posted videos within minutes of each-other? BEST DAY EVER!!!
@modestus2826
@modestus2826 5 жыл бұрын
it makes me feel better about trying things knowing that even the people i look up to make mistakes sometimes
@whale7291
@whale7291 Жыл бұрын
Love how this is now trending cuz of apex
@kittenwillyumz8475
@kittenwillyumz8475 3 жыл бұрын
This was so awesome, I'm going to go ahead and watch something Ive always wondered about... The Myths of Iodine.
@jasonfalzarano7888
@jasonfalzarano7888 5 жыл бұрын
3:44 Forbidden orange juice
@bebanana181
@bebanana181 5 жыл бұрын
Him: it really isn’t that complicated Me: *aRe yOu SuRe AbOuT ThAt?!*
@aldobernaltvbernal8745
@aldobernaltvbernal8745 4 жыл бұрын
Yes
@aldobernaltvbernal8745
@aldobernaltvbernal8745 4 жыл бұрын
I know i'm getting wooshed, but this comment isn't funny.
@bebanana181
@bebanana181 4 жыл бұрын
AldobernalTV Bernal getting wooooshed means that they don’t get a joke, not if they don’t think it’s funny
@rawovunlapin8201
@rawovunlapin8201 4 жыл бұрын
@@bebanana181 indeed - unfortunately that won't stop people from misusing it.
@grain2247
@grain2247 3 жыл бұрын
@@aldobernaltvbernal8745 r/wooOooOOoOSh jk I understand
@moose3306
@moose3306 9 ай бұрын
That bolt thread clip was pretty Frickin neat 👀
@sarcasticnonsense
@sarcasticnonsense 3 жыл бұрын
This popped up on my KZfaq recommended.... I like it and it’s very interesting. I’m subscribing
@kr4ddr0l
@kr4ddr0l 5 жыл бұрын
Hey, I did research on magnetite nanoparticles. In my opinion, the brown thing you get is most likely iron (iii) oxide due to the rapid oxidation under air. Perhaps you can try to do the reaction under an inert atmosphere. Otherwise, play with the ratio, and because iron (ii) will be oxidized, you can try to add more iron (ii). Another suggestion that may be useful is to use charged surfactant as tetramethylammonium hydroxide, and do the coating process under sonicator rather than stirring. It helps to break down the aggregates better than stirring. Good luck!
@Kamizura
@Kamizura 5 жыл бұрын
You are correct. Magnetite is very unstable under oxygen and oxidizes to maghemite, which has its brown colour. But maghemite nano particles still are superparamagnetic and have almost the same saturation magnetization as magnetite.
@jkslvly
@jkslvly 5 жыл бұрын
No one: Absolutely no one: Not a single person: My KZfaq recommendations, at 3 am: Attemptimg To Make Ferrofluid
@freerkelly4103
@freerkelly4103 5 жыл бұрын
Almost 3:00 am
@jadenbucher4002
@jadenbucher4002 5 жыл бұрын
literally 3 am rn
@grizzly5994
@grizzly5994 5 жыл бұрын
Yo its 4:31 for me
@Jess.Maxwell
@Jess.Maxwell Жыл бұрын
2:39 this powder is creating an illusion that it's slightly moving but it's not (pause the video)
@MaryLeighLear
@MaryLeighLear Жыл бұрын
🤯🤯🤯🤯
@devanshvajpeyee8440
@devanshvajpeyee8440 Жыл бұрын
Yooooooo
@ashharjamal5341
@ashharjamal5341 3 жыл бұрын
Woah!!...that was soo cool!👍
@zhengleo6305
@zhengleo6305 5 жыл бұрын
Well at least you tried good job! 👍😀
@IoCalisto_
@IoCalisto_ 5 жыл бұрын
YES KZfaq IS BACK UP!
@IoCalisto_
@IoCalisto_ 5 жыл бұрын
I lied but it's back up now
@KnakuanaRka
@KnakuanaRka 5 жыл бұрын
Yeah, I also had a brief outage around 10. Most obnoxious.
@Amberstargazerofearth
@Amberstargazerofearth 9 ай бұрын
High quality info
@ayosam709
@ayosam709 2 жыл бұрын
This gut took my chemistry grades from f to a+.Thanks man
@zanzzz2481
@zanzzz2481 5 жыл бұрын
0:21 So Satisfying
@nolanjoseph1553
@nolanjoseph1553 3 жыл бұрын
“Mom, can we make ferrofluid?” “We have ferrofluid at home.” The ferrofluid at home: 1:28
@mikecu2249
@mikecu2249 Жыл бұрын
Sure thing Magicman! :D I too have the "stable suspension of magnetaite nanoParticles" , often!
@mayoedstaircase4445
@mayoedstaircase4445 Жыл бұрын
4:24 certified breaking bad moment
@mazidul4902
@mazidul4902 Жыл бұрын
EHEHAHEHAHAHEHAHAHEHE
@kavyachaturvedi6651
@kavyachaturvedi6651 7 ай бұрын
​@@mazidul4902hehehehhehehehhehehhehehehhehehhehehhehehehhehehehehhehhehehehehehhehehehehheheheheheheheheehhehehehehehehhehehehehehhehehhehehehhehehehehehehehhehehhehehehehhehehehhehehehhehehhehehhehehehhehhehehehehhehhehehehhehehehehhehehhehhehehehehehhehehehehhehehhehhehehehehehhehehehehehhehehhehehehehhehehehhheehhehhehehehehhehehhehehehehehhehehehehhehehehhhehehehehhehehehehhehhe........................................
@Alexander_Sannikov
@Alexander_Sannikov 5 жыл бұрын
8:20 when you add oleic acid, overall volume of the fluid noticeably decreases. which's interesting.
@user-nd7rd8jo6h
@user-nd7rd8jo6h 5 жыл бұрын
2:43 Keep the screen paused and shake your phone. The ferro magnetism is not limited to in person interactions. O.o
@nigeldean9820
@nigeldean9820 Жыл бұрын
16:07 looks like him pouring coffee ☕ 🤣
@chrisharten1308
@chrisharten1308 2 жыл бұрын
I was the type of chemistry student that would probably cause an explosion with toenail clippings and water. Yup. I said it. But I love chemistry with a passion and I am really glad I can watch the process from afar. If I was in your lab I'd probably look at something and cause an explosion. Thanks for uploading. Any word on creating Spidey shot yet???
@baao_
@baao_ 5 жыл бұрын
great video, I'd love to see what you'll come up with after further experimenting with it. I am thinking about doing something similar soon
@TheControlPhilosopher
@TheControlPhilosopher 5 жыл бұрын
Hi, I'm an automation engineer from India. Many years ago, I have seen colloidal iron produced by electrolysis in a chemical factory. They were using a electrodes of iron to electrolyse caustic soda! I'm not a chemist & that time it didn't strike me about ferro-fluids. But their product was like bright grey-suspended in paraffin-oil. Is there something relevant for you in my observations?
@heaven4012
@heaven4012 4 жыл бұрын
I looked at ur channel and... you don’t look like an automation engineer.
@mememanfresh
@mememanfresh 4 жыл бұрын
@@heaven4012 Youre stupid
@TAOEXPRESS
@TAOEXPRESS 3 жыл бұрын
@@heaven4012 What job do you have? Whatever it is, you're lying because you don't have videos that make it seem like you have a job! That's the logic you had in that comment, but i hope you've changed since then since it's a comment that was made a year ago.
@notgian_
@notgian_ 3 жыл бұрын
@@heaven4012 *ok lemme just make people know my job is this is KZfaq and hopefully they think that it's my job.*
@popisdeadisagoodsong9997
@popisdeadisagoodsong9997 3 жыл бұрын
@@heaven4012 what... was an automation engineer supposed to look like?
@loaf137
@loaf137 2 жыл бұрын
Out of topic but when he got the powder i got an advertisement of simply piano and i got the most wholesome ad i had ever got that had couples involved in it 😭 ❤️
@isya5372
@isya5372 Жыл бұрын
i love this guy
@Ryan-ju3fl
@Ryan-ju3fl 5 жыл бұрын
if you're on mobile pause at 2:34 and move your screen around
@Kitty-fs4zm
@Kitty-fs4zm 9 ай бұрын
what are you talking about
@Ryan-ju3fl
@Ryan-ju3fl 9 ай бұрын
@@Kitty-fs4zm I dont remember man this was 4 years ago
@kavyachaturvedi6651
@kavyachaturvedi6651 7 ай бұрын
​@@Ryan-ju3fl😂😂
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