Identify chemicals with radio frequencies - Nuclear Quadrupole Resonance (MRI without magnets)

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Applied Science

Applied Science

Күн бұрын

How to build and test an NQR spectrometer, which is similar to MRI, but uses no magnets. NQR frequencies are unique among all tested compounds, so detecting a resonance indicates a near certainty that a specific chemical is present.
Tektronix 2-series oscilloscope: www.tek.com/en/products/oscil... Video capture was done via VNC client
Zeeman effect shifting optical spectral lines: • Candle flame is repell...
Atomic clock calibration using Zeeman effect: • How an Atomic Clock Re...
W2AEW's RF tutorial on quarter wave transmission lines: • #200: T/R Switch w/ PI...
Water deflected by electric field: • How a liquid lens work...
Litz wire only helpful between 50KHz and 1.5MHz - • Resonant Magnet-Field ...
Support Applied Science on Patreon: / appliedscience
Q/A
Why use vacuum variable capacitors? The parallel LC circuit develops well over 1000 volts during transmit, and they are much easier to finely adjust over a large range.
I've spent quite a few hours making this work since late last year. I failed to detect a signal from urea, which burned dozens of hours. Switching to NaNO2 suddenly produced a huge signal.
NQR calculations spreadsheet - docs.google.com/spreadsheets/...
NQR references (many!) : docs.google.com/document/d/1X...

Пікірлер: 1 100
@brunonikodemski2420
@brunonikodemski2420 8 күн бұрын
I built my first NMR machine when I was in high school, in 1960, using the descriptions in a Scientific American magazine. I got an old radar magnet core (with wiring), which allowed a small volume to be magnetized. Winding some sensor coils around this zone, I was able to get a full inversion of several materials, using only an electrometer as a measuring devices. Totally useless to identify much of anything, but clearly showed the principle. This led my algebra/trig teacher to teach me some calculus, since he said I would need it in college. When I got to college I was at least three years ahead of anyone else in my classes, and aced them all. Ended up as an electrical engineer, and later integrated circuits designer. That's the value of real science.
@varshneydevansh
@varshneydevansh 4 күн бұрын
woah
@baloneysaucejohnson8747
@baloneysaucejohnson8747 4 күн бұрын
Homeschooling dad here, you are an inspiration and a blueprint for my little boy.
@HuygensOptics
@HuygensOptics Жыл бұрын
Nice Ben!. Suggestion: in metal detection, they use something called a double D configuration to remove pulse signals completely. Basically you have a separate transmission and reception coil and by strategically placing the reception coil, you can remove the pulse and focus on the signal. This is something you might want to try, because it allows you to remove all the filter electronics from your setup.
@dittilio
@dittilio Жыл бұрын
I assume this set-up you're describing essentially destructively interferes with the carrier signal, leaving the sample signal largely untouched so instead of filtering the noise, you can simply threshold it?
@HuygensOptics
@HuygensOptics Жыл бұрын
@@dittilio no it's about direct cancelling the magnet field. I actually discussed the principle in a video I made some years ago: kzfaq.info/get/bejne/e8mlh9aay7nLcqc.html (around 3.50 min)
@Scrogan
@Scrogan Жыл бұрын
Ah, of course! Very neat idea. I think you’d need to tune each part separately, but at least that’s a lot easier than remaking the output coupling filter. Could even automate a scan using varactors, or those funky current-controlled inductors.
@testboga5991
@testboga5991 Жыл бұрын
It's called induction balance and yes, it works.
@zombieregime
@zombieregime Жыл бұрын
@@HuygensOptics Oh damn! Huygens Optics stopped by! Been following your videos on the mini-monolithic telescope and those dirty lenses. Now I gotta stop by your channel and finally get around to those grinding videos Ive been sitting on watching! Love when these home science on complicated subject channels get together, it makes for an awesome community with a mix of interested amateurs fully invested in everything knowledgeable professionals have to share. And sharing the knowledge its what its all about. Thumbs up to all in the community! You're all awesome, the pros in the know, and the amateurs just looking to expand their knowledge set!😎👍
@frogz
@frogz Жыл бұрын
you make things that people literally study a lifetime for sound easy
@anteconfig5391
@anteconfig5391 Жыл бұрын
That's a good thing. I find that things are often easier than people say they are. If this guy can make something sound easy it's probably 'cause he knows what he talkign about
@accountdeleted3706
@accountdeleted3706 Жыл бұрын
If you can't explain it simply you don't understand it
@bbk9787
@bbk9787 Жыл бұрын
That’s because he is doing it himself and doesn’t have to wade through the constant beating around the bush colleges make you do to get simple information.
@MR-nl8xr
@MR-nl8xr Жыл бұрын
That's because humans tend to make things complicated, especially when you add money with them.
@bigclivedotcom
@bigclivedotcom Жыл бұрын
Ben. Your videos are always ludicrously good. You need to master "shorts" to seed curiosity, then pin a link to the full video at the top of the comments. (Beware - making meaningful shorts about technical subjects is hideously tricky.)
@jonnyphenomenon
@jonnyphenomenon Жыл бұрын
Hi Big Clive!
@hi-friaudioman
@hi-friaudioman Жыл бұрын
Nice to see you here sir.
@MrOlivm
@MrOlivm Жыл бұрын
He needs a forum to have people help draft them. Mmm maybe I should support though patreon and see activity there. Does he even accept support that way?
@jafinch78
@jafinch78 Жыл бұрын
@@MrOlivm Yes, read through the description of this video and you'll find his patreon link. Might be elsewhere found on his channel when clicking on his name and maybe somewhere like in the about section?
@alexlabs4858
@alexlabs4858 Жыл бұрын
Can’t only your subscribers see shorts or did they change that?
@pyromen321
@pyromen321 Жыл бұрын
I just want to say that I really appreciate what you’re doing. Every time you upload a video it’s entirely unpredictable and absolutely fascinating.
@robertsemmler16
@robertsemmler16 Жыл бұрын
ppl who compalin about youtube premium cant appreciate this content. this is priceless.
@ivanpopovic9503
@ivanpopovic9503 Жыл бұрын
During my final year at the university, I was called to be a part of the team designing a real NMR. They gave me the task of designing superconducting magnet. It was very fun, 9 month project that ended with working NMR device, used by chemistry department for structural molecular analysis. It is fascinating that you made working zero field device using only the basic equipment! Great work!!!
@en2oh
@en2oh Жыл бұрын
not sure when you did that, but I was studying Chemistry in the late 1970's. Bruker was our NMR. Brings back old memories - some of which were even quite good! :)
@Bordpie
@Bordpie Жыл бұрын
Back in 2012 I was visiting universities to pick which one to go to and which degree to pick. I ended up touring the physics department at The University of Sheffield (I ended up doing Mechanical Engineering there instead) and I remember them talking about a device to detect the nitrogen or high energy nitrogen bonds (can't remember exactly) in explosives in plane luggage using some technique similar to MRI. I'm guessing it's something similar to this.
@dalehorton7748
@dalehorton7748 Жыл бұрын
Slight error in the diagram, the last 1k resistor to ground on the transmit side actually has another diode pair after it in the practical circuit - which would be essential to not add a 1k load to the sense coil.
@MrOlivm
@MrOlivm Жыл бұрын
A little Diagram/Map Trap to catch the unsuspecting. Good catch!
@w2aew
@w2aew Жыл бұрын
Fascinating stuff as always, Ben. And, thanks for the shout out!
@CuriousMarc
@CuriousMarc Жыл бұрын
This is fascinating. And the DYI wizardry is even more impressive - I didn't know this was even possible! Lots of parallels with the Cesium clock principles, but using the spin of the nucleus instead of the spin of the electron. Even the multi-pulse technique seems analogous to the Ramsey effect used in the clock, where you have two equal interaction regions separated by a period of free precession. And just like you, I also get my RF magic straightened out by watching w2aew's channel!
@batcathatsatchat
@batcathatsatchat Жыл бұрын
The main similarity between the Hahn echo Ben is doing and Ramsey experiments is just that they are both pulsed experiments. Standard Ramsey is limited by T2*, the signal is dead if the space between the pulses is beyond this, whereas Hahn's echo refocuses T2*. You can combine the two, either by reading off the Ramsey signal with an echo (pi) pulse, and/or by inserting a series of pi pulses between the Ramsey pulses to extend the resolution beyound T2*. Ben mentioned T1, but more often than not, T2 (non-refocussable dephasing) is the bigger problem.
@circuitguy9750
@circuitguy9750 Жыл бұрын
This is absolutely amazing! It's incredible to see these very complicated topics explained well and demonstrated on DIY-quality equipment.
@fast_and_curious9144
@fast_and_curious9144 Жыл бұрын
DIY!!
@zombieregime
@zombieregime Жыл бұрын
Lab equipment costing thousands upon thousands of dollars come with precision, repeatability, accuracy, a maintenance plan, and a fancy case. No building filters, or hand tuning, just plop the sample in and hit the go button. But when you understand the mechanisms involved, it really is amazing the kinds of instruments that can be built in a garage that can return useful data! This channel is a great example of what is possible with just some know how and a bloke in his garage!
@zombieregime
@zombieregime Жыл бұрын
@@josseman somethings are unavoidable, also some things are being thrown in the dumpster, or have a simple electrical fault yet being sold 'as parts', or hand me downs, or gifted, or on clearance, etc. Hell, I have a $5000 gilderfluke ride-car controller I acquired through work on theme park animatronics and stage production technology. An expensive piece of equipment doesnt necessarily mean the person who owns it bought it new, or at all. Besides, if you're crafty, you can cover a fair bit of signal inspection with a parallel port and a high sample rate soundcard, or some basic rf/sdr bits and bobs. Sure, a 'real' o-scope, even the cheapest one being sold new, would blow it out of the water. But its technically possible to cover some low hanging bases, just dont expect miracles. Its about using what you can get your hands on. What should they be doing? Judging the waveform by touching wires to their tongue?
@Marin3r101
@Marin3r101 Жыл бұрын
@@josseman how else are you supposed to measure signals accurately? You and everyone and their mother can buy a Oscilloscope, try buying an MRI... You seem like the type of person that can't believe being driven means something."Wow I can't put my head around how you came up with this idea." Or "I don't know how YT Content creators do what they do." This channel may not go into his reasoning for tinkering but human nature is curiosity.
@rrho6701
@rrho6701 Жыл бұрын
@@zombieregime Imagine if a small fraction of the money that the US gifts to foreign countries, were used to set up a few hundred MakerSpace DYI labs across the country, with equipment to loan out like libraries. Where would we be?
@discretegames
@discretegames Жыл бұрын
This is the only channel where I like the videos before watching because I know I'd end up doing it anyway.
@skivvy3565
@skivvy3565 5 ай бұрын
This is the only channel that *Begins with the end results, and showing you. So you stick around due to respect and fascination* . Even all our other favorite channels like tech ingredients and practical engineering are guilty of saddening clickbait and shady tactics
@truegret7778
@truegret7778 Жыл бұрын
That's awesome. When I worked at a cargo container inspection company (using Gamma waves), we were developing device to put in all cargo containers that did a very similar technique. Broadcast, transmit (or chirp), a known spectrum, and a short time later listen to the return. With the return, we have effectively characterized that container. When we cut a small hole (1 ft sq) in the container, the return changed and we detected it. We then know there has been a container intrusion. There is more to the story of what we did after that detection ....
@TheBackyardChemist
@TheBackyardChemist Жыл бұрын
Cocaine?
@c2n10
@c2n10 Жыл бұрын
Gamma Wave? as in human brain waves or Gamma RAY as in ionizing radiation?
@truegret7778
@truegret7778 Жыл бұрын
@@c2n10 Ah, yea, good catch. This was like 15 years ago .... Gamma source. Not sure they still offer the VACIS (Vehicle and Cargo Inspection Systems - port entry, trains, mobile).
@truegret7778
@truegret7778 Жыл бұрын
@@TheBackyardChemist Ha ... no, more like dirty nuc bombs.
@jafinch78
@jafinch78 Жыл бұрын
@@truegret7778 Man, I hope they're performing more samples tested and with better accuracy so no false negatives.
@dario2466
@dario2466 Жыл бұрын
Sometimes I wonder, but yes, I was born in the right time. Thanks to all those wonderful people exploring this world and sharing their insights.
@AlphaPhoenixChannel
@AlphaPhoenixChannel Жыл бұрын
Very cool - For some reason a "low-power-pass" and "high-power-pass" filter is something I'd never even considered. Very cool results! I love that this kind of measurement is home-shop-possible if you're patient
@uploadJ
@uploadJ Жыл бұрын
Its almost like he's designed a RADAR TR tube self-switching system!
@peehandshihtzu
@peehandshihtzu Жыл бұрын
There's no way I would have ever understood any of this coming from a different source, bravo on making it simple enough for a rotten pumpkin to understand. You are a true educator. :)
@BRUXXUS
@BRUXXUS Жыл бұрын
I never know what to expect by a new Applied Science video, but I do know I'll learned something and enjoy the heck out of it!
@NROHK
@NROHK Жыл бұрын
Absolutely amazed at your breadth of experiments. This one was impressive!
@sgravina
@sgravina 14 күн бұрын
This reminded me of my PhD thesis which had a chapter about NQR in Boron and Aluminum. Your explanation was very good and correct.
@drewf64
@drewf64 Жыл бұрын
Wow, not only is it amazing to do NMR without a magnet, this is also one of the best explanations of NMR/MRI I've heard
@mkimball6
@mkimball6 Жыл бұрын
NQR is closely related to NMR, but not the same. NQR is only for quadrupolar nuclei with a decent quadrupolar moment, like 14N and 35/37Cl. NMR without a magnet is more difficult, you basically have to use hyperpolarization
@Zorndar83
@Zorndar83 Жыл бұрын
One reasonable addition to increase the SNR a little could be using a differential amplifier and a pickup coil with two coils of opposing direction (1st ordr gradiometer), that way you could get rid of some of background noise. The passive lambda quarter trick was new to me, I typically work with SQUID detection of NMR signals. Great video!
@pentachronic
@pentachronic Жыл бұрын
Was also wndering if a directional coupler could be used to measure the return signal ?
@stefanm4184
@stefanm4184 Жыл бұрын
I worked on an MRI as an intern for 4 months and never understood how the thing worked despite talking to MRI physicists almost everyday. The way you just explained T1 time and spin echo makes so much sense I can't believe how much I just learned.
@fazergazer
@fazergazer Жыл бұрын
Ben. Echoing Clive’s comment: Your content has always made the most ludicrously complicated subjects accessible. I’d go as far as to say your content is in the top 0.00001% of the KZfaqs for teaching. This is the best description of this practical and theoretical NMR yet. Especially like how you introduce progressive layers of understanding. Like the pulse inversion to rephase the precession. I was struck about how these phenomena have analogous (though not physically arising from the same cause) in optics. Like the phase-conjugate mirror used to demonstrate a laser cavity where one mirror was replaced by a highly non-ideal reflector made from a spatula. The beam automatically tracked the spatula as it was moved about the lab. Anyway, I was a structural biologist and used NMR, x-ray diffraction, and related techniques along with lab-directed evolution using GFP-based folding and solubility reporters, including the “shazam” split GFP tagging systems I developed, now used by other labs to probe the hidden life of molecules in living systems and make new biosensors. I wish your content would have been available in graduate school. cheers!
@tessalittle6244
@tessalittle6244 7 ай бұрын
i have to agree - I've been working with NMR as an analytical tool for a decade went on courses and the last part about pulse sequences and the quadruple aspect is very fascinating and has given me new inspiration to consider approaches like for in the field diagnostics
@ericmichel3857
@ericmichel3857 Жыл бұрын
For a DIY project that actually works it is very impressive! Especially with such limited equipment. I am an MRI engineer so this was right up my alley, and this was a very good layman explanation! A lot of old MR systems get scrapped all the time (even though they usually still work). For just the cost of shipping you could probably get hold of far more powerful equipment.
@SireSquish
@SireSquish Жыл бұрын
This is the guy that bought an Xray tube via eBay and turned it into all kinds of DIY mastery. If he had MRI parts he'd likely build a quantum computer for shits n giggles.
@simoniuszalox3293
@simoniuszalox3293 Жыл бұрын
Hi Ben! You are really trying a physicists solution for the paracetamol issue. May I -as a chemist- give you a recommandation? Your pills mainly consist of filler material and you concentration is low. You will have easy success with an extraction or by synthesizing the paracetamol from scratch. I know tweaking and optimizing is what this channel is all about, but if you want things to be done, do not hesitate to tune concentration instead of circuits. Keep on with your nice work.
@nicolasbrusco1997
@nicolasbrusco1997 Жыл бұрын
Hey Ben, excellent video! I noticed at 13:08 when you showed your physical circuit that one of your diodes in the third stage is backwards! You might get better performance if you fix that I did my senior design project in college on NMR’s, we were trying to design one that could fit in a coffee cup so that ultimately you could send it down an oil well. This video was very informative, it cleared up some things that I didn’t understand even back then. Awesome work
@Jacob_graber
@Jacob_graber Жыл бұрын
The sampling technique you describe late in the video is so mind-blowingly clever, it leaves me in awe.
@ryanfranz6715
@ryanfranz6715 Жыл бұрын
Such advanced science and engineering baked into a single half hour video, yet explained so well I think I might actually understand. I need to go on a walk now to digest all that.
@Muonium1
@Muonium1 Жыл бұрын
Good god, the absolute envy I have for an IQ this stratospherically high..... I recall becoming aware of this so called "zero field NMR" technique perhaps about 2 decades ago, when I believe at the time some kind of start up was trying to commercialize it for abandoned land mine detection. The extreme rapidity with which my total confusion set in when I attempted to understand it at a deeper level perusing the literature was truly humbling. I honestly can't claim to fully understand it now after watching the video either; the best I can hope for, like with most of your beyond-incredible and superbly pedagogically rigorous videos, is hope that a couple crumbs of knowledge might somehow accidentally rub off on me after a few more viewings. Whatever they're paying over at Verily, they probably need to double it. Really looking forward to the follow-up video to this...
@pontifier
@pontifier Жыл бұрын
I'm surprised at how approachable this seems when it's explained well. You make it look easy!
@LuizEnger
@LuizEnger Жыл бұрын
I'm in awe on how complete this video is! Congratulations and thank you for such great content!
@MickHealey
@MickHealey Жыл бұрын
Incredible. Your depth of knowledge is astounding on so many different topics. For me, this one is up there with your digitising the SEM.
@greenbumblebee9687
@greenbumblebee9687 Жыл бұрын
Wow. The longer you have to wait for Ben's videos, the more you can be sure of something awesome is to come 👍👍
@VincentGroenewold
@VincentGroenewold Жыл бұрын
I worked with mass spectrometers and just because I was curious learned about how everything works, helps me a lot in these kind of things where electromagnetism is involved. Awesome video yet again!
@lubos4639
@lubos4639 18 күн бұрын
I admire your capability to explain things - as well as the courage to put this spectrometer together.
@mgdurandolo
@mgdurandolo Жыл бұрын
Your presentations of these complex topics are getting better and better.
@matthewellisor5835
@matthewellisor5835 Жыл бұрын
"...and just the first step of quantum mechanics." he said casually. Another excellent video! Thank you. If like to see any follow-up if you're still working on it. Any ideas why you were having so much more difficult with the paracetamol and why the measured peak did not align with the expected frequency? Perhaps another ingredient in those tablets with a very similar frequency? Again, thanks!
@brocktechnology
@brocktechnology Жыл бұрын
That λ/4 network is startlingly similar the guitar distortion circuits I've been studying lately. While your transmit isolation circuit is also very similar to other distortion circuits, the more stuff you learn, I find the more parallels you find. Kinda magical to see much the same circuit used by one person to make noise(pleasant rock-n-roll noise) and another person to pull a tiny signal out of the noise.
@fryode
@fryode Жыл бұрын
Stuff like this is why I have loved your channel for years, Ben. Life can be a scientific playground and you've proven that time and time again.
@chrisfuller1268
@chrisfuller1268 Жыл бұрын
Amazing!! This is the only video which clearly explains NMR and I have been looking for a clear explanation for years.
@compu85
@compu85 Жыл бұрын
Thanks for making the exploration of this accessible for those of us not in the sciences. Super interesting!
@chemicalvamp
@chemicalvamp Жыл бұрын
You are one of my favorite teachers, always something cool on the whiteboard.
@N.M.E.
@N.M.E. Жыл бұрын
Absolutely insane build Ben! I'm always mind blown with anything RF anyways... it just seems so strange, like some kind of magic in the cursed limbo between electronics and optics
@wowassault
@wowassault Жыл бұрын
It's been about 7 weeks, but youtube finally managed to recommend a new and interesting channel. If only youtube could show me channels like this on a regular basis.
@Gh0sb0ss
@Gh0sb0ss Жыл бұрын
I never thought i'd see a resonance cascade, let alone create one!
@pdrg
@pdrg Жыл бұрын
Thank you, always feel a bit smarter after you release a video, even if that decays away quickly, the fact that I was able to follow along and understand in the moment is testament to the explanation :)
Жыл бұрын
"always feel a bit smarter after you release a video" - I experience the exact opposite of that ;)
@gsuberland
@gsuberland Жыл бұрын
That parallel diode trick is jawdroppingly clever. I figured out the mechanism just a fraction of a second before you explained it and it was a real "Eureka!" moment.
@jbray250
@jbray250 Жыл бұрын
This is legitimately one of the coolest videos that I've seen, absolutely awesome
@jr7853
@jr7853 Жыл бұрын
Your new videos are the best part of my month!
@tommihommi1
@tommihommi1 Жыл бұрын
Those new tek scopes really are a neat form factor, played with them at a trade show a while ago.
@Gaark
@Gaark Жыл бұрын
Never fail to melt my brain man, the stuff you get up to is fascinating
@richardjones38
@richardjones38 Жыл бұрын
What you're able to make garage is amazing. It would not surprise me if one day I browse KZfaq and you've actually come up with a DIY MRI machine!
@ydogprime8389
@ydogprime8389 Жыл бұрын
Hi Ben. At 13:02 when you show a picture of the transmitter isolator it looks like the second from the right diode pair are both facing the same direction.
@simon_far
@simon_far Жыл бұрын
I noticed that too, and was wondering if it didn't matter because the amplifier may have been producing enough voltage to overcome the reverse breakdown voltage of the diode. It would be interesting to know if this was a mistake, and if it may have interfered with his experiment results.
@georgen9755
@georgen9755 Жыл бұрын
what you mean by pair diode ????
@killrb13
@killrb13 Жыл бұрын
RF tech is fascinating! Great video!
@initialb123
@initialb123 Жыл бұрын
so cool, can't even imagine how you decide what project to work on next - love this. Can't wait for more :)
@dangoldbach6570
@dangoldbach6570 Жыл бұрын
This is unreal. I literally was JUST looking at low cost NMR experiments and after reading the white papers for two minutes I was lost, this is literally the clearest explanation of NMR I have ever seen
@jonnyphenomenon
@jonnyphenomenon Жыл бұрын
I was TOTALLY going to say something about how would an alien know what our units of time were, but you beat me to it.
@Muonium1
@Muonium1 Жыл бұрын
We told them what units to use so the Voyager golden record could be decoded correctly. They have to use the hyperfine transition of neutral atomic hydrogen, which we tell them one cycle of which corresponds to 0.7 billionths of one of our "seconds".
@jonanderson5137
@jonanderson5137 Жыл бұрын
Radio wave propagation is black magic.
@WowUrFcknHxC
@WowUrFcknHxC Жыл бұрын
Nope it's definitely light magic 😬🤭.
@shouldb.studying4670
@shouldb.studying4670 Жыл бұрын
@@WowUrFcknHxC that illicited an actual groan 🤣
@Thefreakyfreek
@Thefreakyfreek Жыл бұрын
Agreed
@timnizle1
@timnizle1 Жыл бұрын
😂
@7prudent
@7prudent Жыл бұрын
It is science...
@filipenicoli_
@filipenicoli_ Жыл бұрын
It's always facinating to see your completed projects. They always pack so much knowledge of so many different fields, I can never watch a video without learning something new, be it RF, chemistry, physics or even electronics.
@sirosis1971
@sirosis1971 Жыл бұрын
This is super cool. I understand hardly any of it but you make the concept digestible. Thanks!!
@TheHuesSciTech
@TheHuesSciTech Жыл бұрын
Great work! Years ago, I tried performing NQR on cuprous oxide powder using some custom PCBs, but failed to get a signal. Then my father pointed out that the cuprous oxide would need to be in very pure crystalline form rather than a fine powder; so I basically gave up at that point because recrystallising cuprous oxide seems very difficult. Fantastic to see you succeed; I may well try to resurrect my experiment using sodium nitrite!
@jafinch78
@jafinch78 Жыл бұрын
Maybe you can find a crystallographer (X-ray?) who can work some wonders for you or at least give you some input on how to process the material most effectively. Definitely make a video if you can showing. Will be a neat addition on YT for the World to see. I would like to see at least. This topic and microwave spectroscopy (even the synthetic chemistry) seem like have big gaps in demonstrations on KZfaq.
@hp7033
@hp7033 Жыл бұрын
You're lucky. The most I get out of my dad is suggested improvements to my Goulasch recipe.
@MachiningandMicrowaves
@MachiningandMicrowaves Жыл бұрын
Very neat. I'd probably have gone with PIN diodes and DC bias switching, but the passive approach probably gives enough signal to noise ratio at the expense of needing a bit more power. I'd also consider using either an adjustable pickup loop or a capacitive divider ahead of the receive chain to help increase the tank Q. Very cool solution though, simple and totally self-protecting.
@uploadJ
@uploadJ Жыл бұрын
Carrier lifetimes at 3.6 MHz get kinda iffy for a PIN diide ... standard diodes can be used as switches too, they just require a bit more current to get a low 'ON' resistance'. In the past I've used 1N4148 diodes to switch quartz crystals in receiver and transmitter circuits using either PIN or simple 1N914/1N4148 diodes; PIN at 48 MHz 3rd overtone and simple diode at 12 MHz fundamental frequency.
@manupatet
@manupatet Жыл бұрын
Just repeating these experiments I would consider a personal achivement. Phenomenal content
@tolkienfan1972
@tolkienfan1972 Жыл бұрын
I get excited when I see that an Applied Science video has been posted. It did NOT disappoint! Thank you!
@user-sb3wh3dd4v
@user-sb3wh3dd4v Жыл бұрын
Always fascinating and informative! Thanks!
@williammorris1763
@williammorris1763 Жыл бұрын
I swear you have the most esoteric topics year after year. Keep it up! 🙂
@helicrashpro
@helicrashpro Жыл бұрын
Ben, I've watched your channel for years along with many other science focused channels and I can say confidently that to me you are the most impressive person on youtube. I suppose it's a little like beauty is in the eye of the beholder and your channel to me is the most beautiful orchestration of science hands down.
@db112nl
@db112nl Жыл бұрын
I mainly come here to be humbled, this guy is doing advanced science DIY-style from his garage on a breadth of different topics. I.. installed a fan in my garage today... Amazing content, eloquently explained, even if 5% of this knowledge rubs off on me i would be greatly enriched! Thx Ben
@hammerth1421
@hammerth1421 Жыл бұрын
I didn't know NMR was possible without a strong external magnetic field. This is really cool!
@ivanpopovic9503
@ivanpopovic9503 Жыл бұрын
It is possible, but only in solids. :)
@Muonium1
@Muonium1 Жыл бұрын
there is even such a thing a zero or near zero field MRI. The images are surprisingly usable and comparable at least to the first generation of MRI machine image quality in the early 80s.
@ivanpopovic9503
@ivanpopovic9503 Жыл бұрын
@@Muonium1 As I understand (and here to be honest I'm an electrical engineer and not physicist) You are talking abour near zero field MRI, that is using Earth magnetic fileds? I heard abouth something like that few years ago from a friend who works as a physical chemist and they are using it to immage small lab animals. Quadruple resonance does not need any external field so it is called zero field resonance, and as I remember it is possible only in solids since in fluids the quadruple moment averages out. Again maybe I'm wrong, I have only the basic knowledge in nuclear resonance, my field of expertise is EE. :)
@Muonium1
@Muonium1 Жыл бұрын
@@ivanpopovic9503 yes see the video here "Portable MRI developed at Los Alamos "
@GermanMythbuster
@GermanMythbuster Жыл бұрын
❤❤ *OMG, Ben has made a Video, let me put my life on hold I have to watch this NOW!* ❤❤
@user-yr2nb4vr3q
@user-yr2nb4vr3q 7 күн бұрын
You're a legend man I remember someone mentioning this in the last year of attending uni in 2008 ish and they were promoting it as the future of spectroscopy for airport screening services
@kaezaklimber3391
@kaezaklimber3391 Жыл бұрын
Oh my god. Its people like you who make real youtube's pratical science content advance so much. Thanks immensely, man, I cant even finish this comment of so much gratitude
@elideaver
@elideaver Жыл бұрын
what's with the backwards diode at 13:04? it looks like the third anti noise stage has two facing the same way
@wrekced
@wrekced Жыл бұрын
This part that is open at one freq. and closed at another, reminds me of a book I got from a library in the early '90's about "Pulse Forming Networks". It showed how to design pfn's using coaxial cables and/or passive componnents. I don't remember who wrote it. It had all the formulae you would need to design pfn's.
@thewhitefalcon8539
@thewhitefalcon8539 Жыл бұрын
I heard the Combine use an unusual one with a veeery long rise time.
@MrSomethingdark
@MrSomethingdark 11 күн бұрын
This is one of those videos that just stuns you with what it is. This, my good sir is what YT is all about!!!
@kevinmarr7094
@kevinmarr7094 Жыл бұрын
Great explanation of the classical and quantum physics covering how to drive and receive the signals. Using the gyroscope to show precession made it easy to understand.
@ENDESGA
@ENDESGA Жыл бұрын
I've been learning quaternions and how they work in quantum physics, and this really all makes sense now! Quaternion flipping makes it do into the inverse space and back, so it requires two flips to go back to the original state. I wonder if I can simulate what you talked about with quaternions...
@ButterBallTheOpossum
@ButterBallTheOpossum Жыл бұрын
You really are a next level dude.
@socksincrocks4421
@socksincrocks4421 Жыл бұрын
There isn't a time where you haven't blown my mind. You are my hero. Thanks for all you do.
@bryanpaton
@bryanpaton Жыл бұрын
Such a good/nice video Ben. As someone who works in an MR imaging centre running human experiments you do a great job explaining T2*, T1, de-phasing etc.
@James-yp5dn
@James-yp5dn Жыл бұрын
Dude is crazy smart 🤓
@Kai-ml2iu
@Kai-ml2iu Жыл бұрын
Cool video! The problem of high power transmit pulses coming right back at the VNA is a common problem in the industry. Both radar and telecomunication equipment have to deal with it whenever they want to use the same antenna for Rx and Tx. In the GHz range and above, fully passive devices (so-called "circulators") can be built to seperate the waves depending on the direction they are coming from. In your application, they would not be feasible, unfortunately. However, analog telephones use an opamp circuit replicating that behavior at much lower frequencies. Maybe you would have to use discrete transistors due to the frequency and power requirements, but ultimately it could eliminate the need of replacing the VNA protection circuit each time. The LC tank and matching cap would still need to be tuned, obviously.
@muhammadshahzaib3813
@muhammadshahzaib3813 Жыл бұрын
What i learned in this video is you can bend water with comb. Nice video as always. Thanks for your time. Much appreciated.
Жыл бұрын
I have such high expectations for this channel (way above anything else) and I keep being positively surprised.
@4DRC_
@4DRC_ Жыл бұрын
You should make a little board of just the anti parallel diodes and place it right before the LNA so you have one last crowbar to save you if you have the wrong filter on.
@ThisTrenton
@ThisTrenton Жыл бұрын
Awesome video and always great explanations! If you take suggestions for future videos I would love to see a deep dive on Near-Mid Inferred Spectroscopy of dissolved liquids. It's used in water quality analysis and also in farming for dissolved nutrient analysis and the whole idea is really cool. Haven't seen anything on how to use a measurement like that to quantify concentration in solution so maybe that would be something to think about.
@mr1enrollment
@mr1enrollment Жыл бұрын
with application to hydroponics and the nutrient concentrations
@stephengfazio
@stephengfazio Жыл бұрын
I just picked up a 2 series scope. Now seeing you use it I am even more convinced I made the right choice
@mobilemarshall
@mobilemarshall Жыл бұрын
I have been curious about what a mini home made MRI machine would entail, so this was an especially interesting video. Never heard about this before.
@simon_far
@simon_far Жыл бұрын
For the isolator for the transmit side of the circuit (the pairs of crossed diodes in series) I can see that at 13:05 it looks like one of the pairs of diodes is not crossed but are both facing the same direction. I suppose that the amplifier may be producing a high enough voltage to overcome the diode's reverse breakdown voltage, making it act as a Zener diode, but I was just wondering if that was a mistake or if I am seeing it incorrectly. I love this kind of video though and have learned a lot by watching them!
@veganath
@veganath Жыл бұрын
Yes I noticed that also, he physical has 1 more set[4x] of diodes than on the schematic[3x]. Yes I was wondering the same questions
@yuvalcohen71
@yuvalcohen71 Жыл бұрын
I noticed that one of the diodes on the transmission side filter is reversed (both point in the same direction). I am wondering if this is intentional and if so, why. Otherwise, great video. Thanks
@AppliedScience
@AppliedScience Жыл бұрын
Hah! I'm surprised it works. I'll have to go see tomorrow if it's just a strange lighting effect on video. Certainly looks wrong.
@yuvalcohen71
@yuvalcohen71 Жыл бұрын
@UCeAfLSBX2qycMZDr4siuuAQ 13:03
@simon_far
@simon_far Жыл бұрын
@@AppliedScience Hey, I noticed the same thing. I wonder if the voltage the amplifier is transmitting may be above the reverse breakdown voltage of the diodes you used, making the flipped ones act as zener diodes. This may be why the setup still worked even with this mistake. I'd love to know if this was just a strange lighting effect though, or if not, if correcting it may improve your experiment results. Love your videos!
@robert-wr9xt
@robert-wr9xt 15 күн бұрын
Thanks Ian. You made the world a little better by sharing science with all of us. Be well.
@paulfrindle7144
@paulfrindle7144 5 ай бұрын
For the first time I truly understand nuclear resonance - as the lining up decays after the forming pulse. Your gyroscope precession analogy is perfect. Amazing - thank you :-)
@mikeselectricstuff
@mikeselectricstuff Жыл бұрын
If high Q is important, would Litz wire, or silver-plated wire be helpful?
@AppliedScience
@AppliedScience Жыл бұрын
I thought so too! As it turns out, Litz is only beneficial between 50KHz and 1.5MHz, at least according to the ref that I added to the description. The "proximity effect" eventually becomes worse than the "skin effect". I didn't know this, but thought it was weird that all of the NQR researchers used solid wire for their coils. Silver plating seems like it would help. Plain old thermal noise is also a big problem, and I saw some references using chilled (liquid nitrogen) coils.
@thormusique
@thormusique Жыл бұрын
OMG, I absolutely loved this! I just stumbled upon your channel, which is bloody brilliant, and I'm now a subscriber. Cheers!
@ntwananohaward4504
@ntwananohaward4504 Жыл бұрын
I love your oscilloscope Sir, thanks for diving in depth into this topic.
@Scrogan
@Scrogan Жыл бұрын
Huh, that looks rather different to EFNMR spectroscopy, where I think the characteristic output frequency is dependant on your magnetic field strength. Also I’d have expected litz wire to be better for high Q due to the skin effect, compared to that thick enamel wire. Oh and the second two diodes in your anti-noise amp filter look like they’re both the same way around.
@bradarmstrong1656
@bradarmstrong1656 Жыл бұрын
I found @warecreepers comment about "litz wire...high Q" to be interesting so I asked ChatGPT the following question and got the following agreeable result: me: explain the RF nature of Litz wire used in a coil inductor for high Q at 3.6 ghz ChatGPT: Litz wire is a type of wire that is made up of multiple strands of insulated wire that are twisted together. It is often used in the construction of high-frequency inductors and transformers, as it has a number of advantages over traditional wire constructions at radio frequencies (RF) such as 3.6 GHz. The main advantage of Litz wire is that it reduces the skin effect, which is the tendency of high-frequency currents to flow primarily on the surface of a conductor. This effect is caused by the fact that the resistance of a conductor increases as the frequency of the current increases. By using multiple strands of wire in a Litz construction, the skin effect is reduced, and the current is distributed more evenly across the entire cross-section of the wire. This leads to a reduction in the AC resistance of the wire, which in turn leads to a higher Q factor in the coil inductor. A higher Q factor means that the coil inductor is more efficient at storing energy in the magnetic field, which is important for high-frequency applications such as RF communication systems. Another advantage of Litz wire is its flexibility and ability to handle high current density. This makes it ideal for high-frequency applications, where the current density can be very high. It also allows for a more compact design, which is often a requirement in high-frequency applications. In summary, Litz wire is a type of wire that is made up of multiple strands of insulated wire that are twisted together. It is often used in the construction of high-frequency inductors and transformers because it reduces the skin effect and leads to a higher Q factor in the coil inductor at RF frequencies such as 3.6 GHz, also it has a better current density handling, flexibility and it allows for a more compact design.
@jafinch78
@jafinch78 Жыл бұрын
Speechless! Absolutely total awesomeness. This along with microwave spectroscopy... and maybe a few other spectroscopic techniques when the thought comes to mind, make me wonder really why aren't those methods more well disclosed, taught and used? Neat winter season of experiments on YT. I'm having Les' Lab like thoughts with you demonstrating and teaching a wider range of lab or shop homebrew potentially useful tools; that at the least are awesome to watch you use, better comprehend the system and be aware of the usefulness. I'm also having thoughts of auto tuning those caps with a feedback loop from the NanoVNA I guess firmware... though there are a few apps that can be used to glean the data for a spectroscopy as well as automating some more processes to get more a sweep to characterize unknowns I guess. Probably can use some computational chemistry apps as well to correlate. I suppose my thoughts are turning into some Rube Goldberg molecular energy level states super sweep spectroscopy machine... ideally using the least destructive if not non-destructive methods.
@ardenthebibliophile
@ardenthebibliophile Жыл бұрын
They are known, and taught if you know where to go. It's not more widely used as it's limitations make it applicable for niche scenarios only
@MrFraneque
@MrFraneque 6 ай бұрын
I must say that again. You are the neighbour I always dreamed to have. Thumbs up always, following and supporting since the beginning. Ben, your master videos are inspiring. I LOVE them all. Keep on going!
@peterwilson7532
@peterwilson7532 Жыл бұрын
This is a fascinating and unique channel. You deserve all your success and more. Just had to subscribe.
@tufan__1048
@tufan__1048 Жыл бұрын
citizen scientist at his best.
@tufan__1048
@tufan__1048 Жыл бұрын
Hi Ben.,did you recognize the scam here?
You can mix 10 marbles until they sort themselves. Why not 100?
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I tried to make a camera sensor
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