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@ravenj2400
@ravenj2400 5 күн бұрын
🤓 i’m excited 🤓
@plenty1347
@plenty1347 2 ай бұрын
It works, but I have to prepare electroless copper solution each time. In your guide you say that I need to acidify it after use with H2SO4 and make it basic using NaOH when taken out of storage before next use. Can you provide exact pH values?
@s.sradon9782
@s.sradon9782 2 ай бұрын
Would you consider making a video on the synthesis of electroluminescent phosphor? It is a very cool technology.
@mirzahosein2261
@mirzahosein2261 3 ай бұрын
you are smart man, great work..
@ComradNoFucksGivin.
@ComradNoFucksGivin. 3 ай бұрын
That's how a car horn works.
@ahmadzoghi338
@ahmadzoghi338 3 ай бұрын
Niceeeeeeee🔥
@boriscat1999
@boriscat1999 3 ай бұрын
great hack. thanks for sharing!
@Obliterous
@Obliterous 3 ай бұрын
Its even tuneable if you add some mass to the cone.
@hydrogentime2872
@hydrogentime2872 3 ай бұрын
If you're curious what does the waveform looks like I measured it with an oscilloscope kzfaq.infoUgkx-uD0CHLhRvanLAB8pf57c0F2gAFuoBfC
@bpj1805
@bpj1805 3 ай бұрын
I was half expecting you to reveal a small relay behind the speaker cone when you turned it over. (Relays by themselves can be wired as buzzers, of course.) I don't know if a relay counts as an active device.
@hydrogentime2872
@hydrogentime2872 3 ай бұрын
In a way it is a relay, its just sharing the coil and part of the contact with the speaker.
@techticks5274
@techticks5274 6 ай бұрын
Is this palladium based activator solution and electroless copper bath stable and can be used for months? If not then how manufacturing factories use this solution for long time?
@hydrogentime2872
@hydrogentime2872 3 ай бұрын
If you keep it in a well sealed container the activator is stable for years. When the activator goes bad it also changes color becoming transparent, so it's easy to know if it's still good.
@user-kn5dn1kf3d
@user-kn5dn1kf3d 6 ай бұрын
From Iraq 🇮🇶
@mernokimuvek
@mernokimuvek 7 ай бұрын
Nice experiment. I had the idea to put lithium in a tube, seal it and create a low pressure discharge tube without a vacuum pump. Only argon, hydrogen and ammonia(from lithium nitride reacting with water vapor) should be left.
@hydrogentime2872
@hydrogentime2872 3 ай бұрын
At high temperatures lithium may react with the glass though, not sure.
@dawidbrzeski6096
@dawidbrzeski6096 7 ай бұрын
Your process is very expensive because you use pdcl2. I have another solution to use AgCl for activator.
@rubenfigueredo2507
@rubenfigueredo2507 6 ай бұрын
Can you share it please?
@hydrogentime2872
@hydrogentime2872 3 ай бұрын
Post a link to your procedure? I'm curious.
@muhammadasjad3416
@muhammadasjad3416 7 ай бұрын
please tell me is the palladium activator solution colloidal or a well mixed solution?? yours looks well mixed but I have tried it is always colloidal.....kindly clarify
@hydrogentime2872
@hydrogentime2872 3 ай бұрын
I'm not sure. The dark color could be a fine suspension of metallic palladium but I did not investigate.
@Mikkel324
@Mikkel324 7 ай бұрын
Nice tube! I did something very similar using titanium wire to act as both a feedthrough and to capture residual gas by sputtering. Titanium happens to be pretty well matched to soft glass when it comes to expansion, making it pretty simple to create good seals. www.dropbox.com/scl/fi/zq9pqlwfj9c97pr1ohukd/2021-10-08-23.14.52.jpg?rlkey=g6nkuw43651zwmnu1annhoaau&dl=0
@WaffleStaffel
@WaffleStaffel 7 ай бұрын
Very cool. I didn't know you could use magnesium as a getter so easily, good to know!
@andymouse
@andymouse 7 ай бұрын
Neat....cheers !
@user-yb5cn3np5q
@user-yb5cn3np5q 7 ай бұрын
Thanks for sharing! Also that's already halfway to He-Ne laser, y'know...
@mpelagio-engenharia
@mpelagio-engenharia 7 ай бұрын
The yellowish collor of the Paladium Solution is because the chemicals in the solution are reducing and they need to be completed again to original levels.. normally adding some more Palladium regularly... there are some lab tests to detect what needs to be added to solutions be its a little complex to explain here...
@the_runofff
@the_runofff 7 ай бұрын
incredible process, im really frustrated with my boards not having hole plating. thanks so much for this!
@hydrogentime2872
@hydrogentime2872 7 ай бұрын
Be careful if you try to replicate this, you need to have some chemistry experience and a fumehood
@Cristi0986
@Cristi0986 8 ай бұрын
I miss chemplayer background song ❤
@gilbertogrimm5843
@gilbertogrimm5843 8 ай бұрын
Acido ascorbico , precipita la plata?.
@fouzaialaa7962
@fouzaialaa7962 9 ай бұрын
for electro plating use a coffee filter and wrap the anodes in it to catch the large chunks of copper (do not wrap the PCB) i myself use a laser to etch double sided pcbs , i use flatcam and Lightburn to generate the cnc job , i then take a cheap pcb with copper already in it , coat it in spray paint ,and then burn the negative of the traces of the pcb on both sides with the laser , then i etch it ,and give it a green coat of paint like a solder mask , and then burn away the green paint to reveal the solder pads . its less involved since im bad with chemicals ,my reason for doing this is that shipping from pcb way or any other company is 25 $ plus so i just do it at home
@hydrogentime2872
@hydrogentime2872 7 ай бұрын
Turned out the main issue was the excessive resistance of my alligator clips resulting in the two copper electrodes having appreciably different potential and trying to electroplate between them.
@user-yk9vr4vy5l
@user-yk9vr4vy5l 3 ай бұрын
Graphite spray ,scrap and Sand,electrocopper,Holes are metalised...tyour laser Paint système I use too,but m'y lasers ends After a total of some hours of engraving...and i dont know why....maybe IS thé common supply of the laser with Steppers 12 v...some surges maybe during motions
@ABehrooz
@ABehrooz 9 ай бұрын
Hello, Are there any substitutes for PdCl2? I can't find it at an affordable price where I live. (the only seller charges an arm and a leg for a gram of it)
@hydrogentime2872
@hydrogentime2872 7 ай бұрын
There is no substitute that I know of for this process, but search on youtube for other processes. Some had success spraying conductive carbon paint and then electroplating onto that.
@ABehrooz
@ABehrooz 7 ай бұрын
@@hydrogentime2872 I pulled the trigger and bought everything for this process. (Except the PdCl2, of course). I'm trying to find another supplier for it, fingers crossed. I'll post results when I actually get to do it on a real job.
@bluskyy5755
@bluskyy5755 9 ай бұрын
An it would have been Educating if we told an shown what was the liquid in the little Amber bottle that you mixed with the Sulfur. You turned the bottle around so the label was hidden. I couldn't understand most what you were speaking. 😢
@hydrogentime2872
@hydrogentime2872 7 ай бұрын
The solvent is xylene. It is also written in the initial safety notice.
@CrayzxxXxx
@CrayzxxXxx 11 ай бұрын
do i need both electroless and electrolythic copper plating for connecting vias or can i just use one of them
@hydrogentime2872
@hydrogentime2872 7 ай бұрын
You can in theory use only electroless, but it is slow to build up the desired copper thickness, and you need to fine tune the process for the surface finish to withstand the etching. Only electrolytic does not work as copper only plates to already conductive surfaces, and the holes are not conductive initially.
@skeeviesteve1071
@skeeviesteve1071 11 ай бұрын
... Love to see more ideas with glass
@mpelagio-engenharia
@mpelagio-engenharia 11 ай бұрын
The Paladium Activator sometimes turns to a yellowish transparent collor... this case You just put it inside a glass flask and this flask inside another conteiner (or a Pan for example) with boiling water for some 20 minutes, 30 minutes until the solutions turns to dark brown collor... I have made it to a lot of solutions of Paladium and it worked very well..
@hydrogentime2872
@hydrogentime2872 7 ай бұрын
Will try next time it happens
@AlbertoMelappioni
@AlbertoMelappioni 11 ай бұрын
Bello! Non vedo l'ora di vedere il tubo riempito di Neon. A che tensione lavora l'alimentatore?
@hydrogentime2872
@hydrogentime2872 7 ай бұрын
Open circuit it overflows my oscilloscope, and the frequency is too high for a multimeter. I need a 100x probe...
@nikolaiturcan6963
@nikolaiturcan6963 11 ай бұрын
Do you know why the lamp makes these discrete lines? That increase in number as the pressure increases, and have this "stepping" behavior (appearing or disappearing 1 line at a time) ?
@AlbertoMelappioni
@AlbertoMelappioni 11 ай бұрын
The phenomenon is called plasma striations or plasma stratification. It's quite complex. When we are in a DC discharge, a bright anode column is formed at a certain pressure spaced out by a dark area. At lower pressure ranges, the positive column is composed of striations, or ionization waves, caused by the electrons finally having enough energy to ionize the gas, then losing the energy by ionizing it, then reaccelerating back to high enough to repeat. This causes a series of barrages of photons being released in waves, seen as striations in the plasma. In AC the anodic column moves continuously and makes the phenomenon even more complex and susceptible to other stimuli such as capacitive coupling, any resonances between the frequency and the ionized gas, etc.
@andymouse
@andymouse 11 ай бұрын
Also known as 'Faraday or Crookes' Dark Space and is as you say, very complex.@@AlbertoMelappioni
@hydrogentime2872
@hydrogentime2872 7 ай бұрын
Learned something new. Thanks.
@zodd0001
@zodd0001 Жыл бұрын
You are ever one step forward but you should make videos more frequently.
@Jhonsket82
@Jhonsket82 Жыл бұрын
Subtitle nobtranslate sir😢
@Pubgfiregamingop
@Pubgfiregamingop Жыл бұрын
sir thank you so much for making this love you so much plz one question Sir i made zinc sulphide with NA2S+ZNSO4= NASO4+ZNS CAN I USE IT TO MAKE GLOWING POWDER PLZ TELL SIR
@hydrogentime2872
@hydrogentime2872 3 ай бұрын
Never tried this reaction. Assuming it does indeed make ZnS, you'll need to filter and dry the ZnS, and then proceed as in my video adding the desired dopant such as CuSO4 and fire it in a quartz tube furnace for it to glow.
@nikolaiturcan6963
@nikolaiturcan6963 Жыл бұрын
Bel Canale! Continually cosi!!!
@aletatianny18
@aletatianny18 Жыл бұрын
👏
@lifeitsnotfun
@lifeitsnotfun Жыл бұрын
based
@ue8853
@ue8853 Жыл бұрын
Why is a quartz tube required to dope the zinc sulfide?
@hydrogentime2872
@hydrogentime2872 Жыл бұрын
All other types of glass, including borosilicate, will melt way before the desired temperature is reached.
@MH-GoL
@MH-GoL Жыл бұрын
Nice Video, thank you very much! After many years of using "Toner Transfer" to make my pcb i now bought a UV DTG Printer and directly print the mask for the design on the board. After etching i print the "soldermask" to the pcb too. The only thing i need to get done now are the vias. Your solution looks perfect but i'm a bit worried about the Formaldehyde. I'm not a chemist, is it possible to replace it with a less toxic ingredient? Triton-X100 is even a problem in the EU, it is banned by REACH since 2021. Is there an alternative available?
@hydrogentime2872
@hydrogentime2872 Жыл бұрын
The Triron-X100 could probably be replaced by another surfactant if you can't find it, but some experimentation may be required. Formaldehyde is very hard to replace, there are alternatives which are known to reduce copper salts to the metal in a controlled way but are just as toxic. If you have no chemical experience I suggest to either wait for someone to develop a safer process (NurdRage was trying for example), or to learn chemistry one step at a time before messing with formaldehyde. And build a fumehood.
@user-ho7vh5cp8e
@user-ho7vh5cp8e Жыл бұрын
Hello! Very cool! The same phosphorus is used in alpha radiation detectors?
@hydrogentime2872
@hydrogentime2872 Жыл бұрын
I'm not sure it's the exact composition. There are many green emitting phosphors.
@almanimaxim4223
@almanimaxim4223 Жыл бұрын
did you test your vias with current? i found it very useful to do this test in the developement of my process my 0,3mm vias usually can take about 5A, 1,2mm vias could conduct even more then 25A of current with a test batch and the vias fusing at about much lower currents, i found it useful to use that as an indicator also it turns out: you can fairly use a lot of other colloid solutions for activation (even copper in NaBH4 itself), it requires an additional etching and desmearing step+ sensitation steps tho
@hydrogentime2872
@hydrogentime2872 Жыл бұрын
Interesting suggestions, I did not test the vias to failure with current, but I made a few boards since I shared the process and all of them are still working fine. My smallest vias are 0.5mm. I'd be interested if you shared (maybe in a video?) your NaBH4 activation process, I don't have that chemical in my lab, but if it turns out to be useful I may try to get some.
@rubyledger7549
@rubyledger7549 Жыл бұрын
Thanks for the detailed video, we are making this today in my physics university class. Please could you let us know if there is a way to make the ZnS:Cu into a paste/liquid to make it stick to the bottom of a glass conical flask to form a phosphorescent screen (without dripping down the sides if it is moved around). We are making a DIY cathode ray tube :)
@hydrogentime2872
@hydrogentime2872 Жыл бұрын
Chapter 5 of the book Inorganic Phosphors lists some methods. You can find the book in this thread www.sciencemadness.org/whisper/viewthread.php?tid=142184&page=2
@rubyledger7549
@rubyledger7549 Жыл бұрын
@@hydrogentime2872 Thank you !
@Pubgfiregamingop
@Pubgfiregamingop Жыл бұрын
@@hydrogentime2872 sir thank you so much for making this love you so much plz one question Sir i made zinc sulphide with NA2S+ZNSO4= NASO4+ZNS CAN I USE IT TO MAKE GLOWING POWDER PLZ TELL SIR
@hydrogentime2872
@hydrogentime2872 Жыл бұрын
@@Pubgfiregamingop assuming you made zinc sulfide, yes, you can make glow powder if you follow the process described in the video. You will need to add a tiny amount of copper sulfate and ammonium chloride, and heat the powder in a furnace.
@sumguysr
@sumguysr Жыл бұрын
Can this process work with electroless nickel solution?
@hydrogentime2872
@hydrogentime2872 Жыл бұрын
I'm not sure traditional copper etchants can etch nickel too, if they don't you'll have problems at the final etch stage. I know nickel plating is used after copper plating when PCB gold plating is needed, as gold plating directly over copper is troublesome, but I think this is done after etching? Not sure, if I ever try gold plating I'll give more thoughts to the application of nickel chemistry to PCB manufacturing and maybe make a video. No plans yet, though.
@behzadabf
@behzadabf Жыл бұрын
very well describe.. thanks a lot sir.
@user-yb5cn3np5q
@user-yb5cn3np5q Жыл бұрын
A always wondered how those vias are made. Thank you so much!
@hydrogentime2872
@hydrogentime2872 Жыл бұрын
No problem!
@user-yb5cn3np5q
@user-yb5cn3np5q Жыл бұрын
I wish it was easier to find such channels.
@aaronjennings8385
@aaronjennings8385 Жыл бұрын
Needs subtitles
@AppliedCryogenics
@AppliedCryogenics Жыл бұрын
Maybe it would be easiest to make a cathode ray tube with some of your phosphor inside. With your original approach, maybe a good dielectric between the phosphor-coated conductive glass and the electrodes would act like a capacitor and allow you to use a higher electrical potential.
@hydrogentime2872
@hydrogentime2872 Жыл бұрын
I am learning (simple) glassblowing for another project so it may be a good idea, but it won't happen soon, as I currently lack the high vacuum equipment needed for making a CRT.
@AppliedCryogenics
@AppliedCryogenics Жыл бұрын
Thank you for the interesting video. I always wondered how copper doping could be achieved at home to make green phosphor. I'm definitely going to watch the next video in the series.
@hydrogentime2872
@hydrogentime2872 Жыл бұрын
The series is currently on hold as I failed to make a red phosphorescent material, and then moved to doing other stuff. Would like to get back to it someday, though.
@dogodogo5891
@dogodogo5891 Жыл бұрын
hi check out this link kzfaq.info/get/bejne/j996mbWJ0NGRoGQ.html i suspected blue n green are sufate n chloride of copper but iam not sure about reducing agent(ascorbic acid/sugar maybe?) but there are other strange ingredients i think ammonia / Naoh, n some sensitizer not based on noble metal, what do you think?