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NMR Analysis - Predicting a Structure Based on NMR and IR Spectra

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Tony St John

Tony St John

Күн бұрын

Пікірлер: 58
@TonyStJohn
@TonyStJohn 6 жыл бұрын
For a copy of the tables I use click here: drive.google.com/file/d/0BwOceMKQTVFxRTh1Szl4aTh0eE0/view
@jibuttu
@jibuttu 2 жыл бұрын
Thank you, how do I contact you directly
@princessmallo2161
@princessmallo2161 Жыл бұрын
It says I require access to the folder can you please do that
@EcExplorer
@EcExplorer 6 жыл бұрын
1. I think the very first step should be measuring the degree of unsaturation. 2. For ensuring which one is e/f, you can go for chemical shift calculation.
@MrViniWilliams
@MrViniWilliams 7 жыл бұрын
Man, I just found your videos and they are really good, you talk very clearly and show every step of the thinking behind the problem. I was searching for videos like that so I could see someone actually working on determining structures from spectra and it helped me a lot. About the UV, it's probably just confirming the existence of conjugation, I think. The more conjugated the molecule, the higher the max wavelength it absorbs in UV-VIS region. The spectra shows an absorption at 260 nm, so it must have some conjugation, but not too much as it falls in the UV region, not in the VIS.
@kconley7043
@kconley7043 2 жыл бұрын
Kkkii
@kconley7043
@kconley7043 2 жыл бұрын
MMA
@kconley7043
@kconley7043 2 жыл бұрын
Aid
@kconley7043
@kconley7043 2 жыл бұрын
It doesn’t matter what it was good 😊 but I love ❤️ so you know me lol 😆 just let us keep
@SquatSimp
@SquatSimp 4 жыл бұрын
2:30 that’s something called “overtone” created from the carbonyl
@bsavvy5450
@bsavvy5450 6 жыл бұрын
This was really helpful thanks, maybe running through how to get the Molecular formula when you don't have it would be a plus
@kconley7043
@kconley7043 2 жыл бұрын
U
@kconley7043
@kconley7043 2 жыл бұрын
Oh
@kconley7043
@kconley7043 2 жыл бұрын
Huge
@kconley7043
@kconley7043 2 жыл бұрын
It was a little bit zdfggg but D but
@kconley7043
@kconley7043 2 жыл бұрын
Our
@justinlee6747
@justinlee6747 3 жыл бұрын
The small peak at 3400 in IR is the overtone from the carbonyl.
@mingmingdai9801
@mingmingdai9801 4 жыл бұрын
It's quite brilliant!!! Thank you for sharing. Regards from China
@satevamarie3597
@satevamarie3597 4 ай бұрын
The peak at 122 on MS is called a McLafferty rearrangement and it includes a loss of a whole molecule ( a neutral molecule fragmented off). 😊
@ConnectSparrows
@ConnectSparrows 7 жыл бұрын
This video was very helpful! Thank you for sharing your wisdom and time!
@abassseidu9862
@abassseidu9862 Жыл бұрын
God bless you....I’m now loving organic chemistry 😊🎉❤
@Bripirate
@Bripirate 6 жыл бұрын
My only criticism is that it would be nice to see the NMR data listed out....2H (triplet), etc. along with the actual chemical shift data.
@alighaddar3076
@alighaddar3076 3 жыл бұрын
That was pretty helpful. Though you can note that an odd electron ion or an even mass fragment (here it’s at m/z 122) formed through fragmentation of an even mass molecule would result from a rearrangement. This rearrangement here is McLafferty concerted rearrangement that would happen when a gamma sp3-hybridized carbon has a hydrogen atom that transfers to the heteroatom (here it’s the oxygen) with alpha-beta bond to the double bond being cleaved. Note that for an ester it’s a special case rearrangement considering the oxygen atom of the alcohol chain to be alpha with respect to the double bond. Hope this helps.
@huyenphong1840
@huyenphong1840 7 жыл бұрын
thanks for your useful video. I will have an exam on friday, this video is awesome
@TonyStJohn
@TonyStJohn 7 жыл бұрын
Great! Glad to hear it and good luck on Friday!
@brownytracyrsa1928
@brownytracyrsa1928 3 жыл бұрын
Very helpful 😊😊😊I'm like Organic is my favorite right now 😊🔥🔥🔥💃💃💃
@aratimaurya8464
@aratimaurya8464 5 жыл бұрын
i have confusion about CH splitting ?? ....
@roisatulfitri6986
@roisatulfitri6986 4 жыл бұрын
Matur nuwun nggih pak. Kula dados ngertos amargi panjenengan 😊
@Maria-db7px
@Maria-db7px 5 жыл бұрын
Thanks for sharing, it helped me a lot!!! regards from Spain!
@austinjnrkumwenda8620
@austinjnrkumwenda8620 Жыл бұрын
Good explanation, thank you Sir
@eeanas
@eeanas 7 жыл бұрын
good young man , wish for you all the good
@NganNguyen-ng1nn
@NganNguyen-ng1nn 7 жыл бұрын
hi, it would be really useful if you could include pdf of those chart
@akirauzumaki3805
@akirauzumaki3805 2 жыл бұрын
Really a great video! Thanks!
@khanzada6755
@khanzada6755 2 жыл бұрын
It was very nice lecture.
@alexisgeneve2471
@alexisgeneve2471 4 жыл бұрын
This doesn’t explain why you think the ways that you do! During the video you should be explaining why you came to those assumptions
@kurufunda
@kurufunda Жыл бұрын
That is a very usefull video thanks from Türkiye💌💌💌
@fatihokhider
@fatihokhider 5 жыл бұрын
Thanks...good structure determination detective work...cheers
@zzia.official
@zzia.official 6 ай бұрын
Thank you
@plamenpenchev262
@plamenpenchev262 2 жыл бұрын
The peak you are wared about around 3350 is the overtone of C=O
@muhammadnaeembashir830
@muhammadnaeembashir830 2 жыл бұрын
This is really helpful thank you so much sir
@zurtalabkhan8952
@zurtalabkhan8952 Жыл бұрын
Thanks
@muhammadnaeembashir830
@muhammadnaeembashir830 2 жыл бұрын
Sir also include CNMR spectrum with these two spectrums
@milonmohanta810
@milonmohanta810 2 жыл бұрын
It seems you did not assign the carbonyl carbon in C-NMR!
@muhammadnaeembashir830
@muhammadnaeembashir830 2 жыл бұрын
Hello sir I'm from Pakistan..I want to ask about the solving all the spectrum with concluding result..I mean I want to use iR,HNMR,CNMR and Mass spectrum to conclude structure
@yendavarunkumar6824
@yendavarunkumar6824 5 жыл бұрын
thanks from india
@amitkhandelwal9074
@amitkhandelwal9074 Жыл бұрын
Sir i have an NMR data of my sample can you interpret it?.
@john.the.beloved
@john.the.beloved 5 жыл бұрын
Thanks a lot, Sir
6 жыл бұрын
hello can I get you chart for IR and H NMR or all what you have ?
@TonyStJohn
@TonyStJohn 6 жыл бұрын
Hello! For a copy of the tables I typically use click here: drive.google.com/file/d/0BwOceMKQTVFxRTh1Szl4aTh0eE0/view
@noor-or8kw
@noor-or8kw 7 жыл бұрын
the aromatic region should show 4 lines instead of 3 ?! 1 more for the carbon connected to the ester carbonyl?!!!
@TonyStJohn
@TonyStJohn 7 жыл бұрын
Are you referring to the carbon NMR? Since this is a DEPT experiment, only the carbons that have H's bonded to them are showing up. It is not a normal carbon NMR! Hopefully this answers your question?
@noor-or8kw
@noor-or8kw 7 жыл бұрын
got it , thanks a lot i find your videos very helpful
@riyadh4u138
@riyadh4u138 7 жыл бұрын
I need some help, Is there anyway I could communicate with you Tony?
@TonyStJohn
@TonyStJohn 7 жыл бұрын
Hi Amal! You can email me at: Tony.ChemistryExplained@gmail.com
@dipakjadhav9624
@dipakjadhav9624 4 жыл бұрын
Hi sir This is Dipak from india Please give examples on TOCSY AND COSEY Spectra
@rociolopezdomene9567
@rociolopezdomene9567 6 жыл бұрын
THANK YOU:D
@chemistrywithadityabhaiya7920
@chemistrywithadityabhaiya7920 3 жыл бұрын
Please solve on C14H15N
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