Preparing a platinum catalyst for the Ostwald-Oxidation feat. aqua regia

  Рет қаралды 20,202

Astral Chemistry

Astral Chemistry

Күн бұрын

In this video, we show you in detail how to make a platinum contact that is suitable for the Ostwald-Oxidation of ammonia to nitric acid. Enjoy!!
Ostwald Oxidation: • Ostwald process: Catal...
Music: "Hitman" by MacLeod, licensed under Creative Commons Attribution license (creativecommons.org/licenses/...)
Source: incompetech.com/music/royalty-...
Interpret: incompetech.com/

Пікірлер: 64
@mystermisterairy6257
@mystermisterairy6257 5 жыл бұрын
Hands down, one of the best chemistry/science videos i have ever seen. Nice work. The music was spot on. W special emphasis to the pipette filtration segment as well as the dissolving of the residue in the bowl w the stirrer going . Thank you Astral 💚
@jerrywbrice
@jerrywbrice 4 жыл бұрын
Extremely useful material here. Surely appreciate it!
@cobalt7530
@cobalt7530 6 жыл бұрын
Amazing!!!! You are the first amateur chemist I have seen attempt this!! This catalyst is so cool and I have been wanting to have some for quite a long time.
@astralchemistry8732
@astralchemistry8732 6 жыл бұрын
Thank you very much!
@astralchemistry8732
@astralchemistry8732 6 жыл бұрын
First! :P We discovered that we have been running a lab for years without having sodium chloride. But a good chemist always has some sodium and chlorine gas, am I right?
@joehill2420
@joehill2420 6 жыл бұрын
Thank you for your high quality videos. A joy to watch.
@astralchemistry8732
@astralchemistry8732 6 жыл бұрын
Thank you very much. After a year now we start to figure out how editing works.
@snowdaysrule
@snowdaysrule 6 жыл бұрын
This is so cool!!! I've been doing a lot of experimenting with platinum catalytic propane heaters lately, and I've always wondered if it would be possible to make one myself. After watching your video it definitly appears to be feasible! A friend of mine recently opened up a small automobile catalytic converter with an acetylene torch, and obtained the ceramic honeycomb inside. When I decide to chemically process it, instead of trying to obtain a bead of the metals it contains I may just keep them in solution and apply them to some quartz wool like you did here. Thanks for the inspiration!
@grunthostheflatulent269
@grunthostheflatulent269 6 жыл бұрын
Thank you for showing us this process and your methodology! Pt is a pretty mysterious and amazing element.. Put a Pt/Nb sheet in a wood smoke stream and you can smell all the transformed compounds produced by it (consumes it, though..)
@nedshead5906
@nedshead5906 2 жыл бұрын
I've finally got everything I need to try this, the last piece of the puzzle was the platinum, which I found in a broken R type thermocouple in a skip bin, from what I've read the negative leg is 100% platinum and the positive leg is 87% platinum/13% rhodium
@WaffleStaffel
@WaffleStaffel Жыл бұрын
Nice find! Just imagine how many tons of gold are sitting in landfills.
@ColinRies
@ColinRies 6 жыл бұрын
Really nice video. I'd just recommend you adapt the volume of music and voice a bit, when the music comes, I have to turn down the volume so much that later I can't hear the voice...
@nattsurfaren
@nattsurfaren 6 жыл бұрын
Awesome video!!!
@astralchemistry8732
@astralchemistry8732 6 жыл бұрын
Thanks!!
@AllChemystery
@AllChemystery 6 жыл бұрын
nice job/ used far less matal than i imagined
@astralchemistry8732
@astralchemistry8732 6 жыл бұрын
Thank you very much!
@Andrew-my1cp
@Andrew-my1cp 4 жыл бұрын
Hi! Great channel! What hot plate stirrer do you use or recommend? I'm torn between hot plates and people give mixed reviews.
@richardlangstaff6358
@richardlangstaff6358 3 жыл бұрын
Is it possible to use aluminum silicate ceramic wool in stead of the quartz wool?
@geoffc1694
@geoffc1694 5 жыл бұрын
Hi have you considered using a tilly lamp mantle thats 99% thorium dioxide as a catalyst? that was the other catalyst used industrially when pt ran short in ww1. my research gives 11 parts ammonia gas 89 air run through preheat 700c and use gasflow to push the exothermic catalyst temperature to 800-850c. Above 900, selectivity is reduced. thorium ran at atmospheric pressures, pt 4-5atm. 2 cooling chambers are used, 1 has water vapour added, one has o2. but we can use h2o2 bubbler instead. Apart from its fragility i think the tilly lamp mantles may be ideal, for surface area and contact times, easy to apply and clamp to a tube etc
@Taha-hv6yj
@Taha-hv6yj 4 жыл бұрын
Nickel and Cobalt can catalyze the oxidation right?
@Tridenux
@Tridenux 6 ай бұрын
What should be the concertation of nitric acid ? And other acids you used ?
@Pyrokartoffel
@Pyrokartoffel 2 жыл бұрын
Can i use small alumuminum oxide balls instaed of quartz wool?
@2mc29
@2mc29 4 жыл бұрын
killer intro!
@mixdxperience1000
@mixdxperience1000 2 жыл бұрын
can i do this via kcl and potassium hexachloroplatinate?
@karolus28
@karolus28 3 жыл бұрын
cool
@embuscadosmetais
@embuscadosmetais 2 жыл бұрын
I think you can help me, can the rhodium chloride precipitated in water regia be taken directly to melting with a blowtorch? palladium I've already got it, but rhodium hasn't.
@user-un7sq5bf2d
@user-un7sq5bf2d 2 ай бұрын
جرب العمل في القواعد اعتقد ستذيبه بالكامل
@TheChemicalWorkshop
@TheChemicalWorkshop 6 жыл бұрын
Big thumbs up for showing the process, we are currently purifing crude platinum for exactly this process (But we need a lot of time for editing...) But please make your videos a bit shorter and to the point if you can (:
@astralchemistry8732
@astralchemistry8732 6 жыл бұрын
Thank you for your opinion.
@kelvinpino4065
@kelvinpino4065 3 жыл бұрын
Hi I tried to replicate the experiment but I didn't work, the resulting platinized quartz wool doesn't catalize the combustion of my burner, I really appreciate your help
@Jeanpaul465
@Jeanpaul465 6 жыл бұрын
Is it possible to use the same route,to produce a gold catalyst?
@kelvinpino4065
@kelvinpino4065 4 жыл бұрын
I think that gold have no catalytic properties
@thesciencefurry
@thesciencefurry 3 ай бұрын
I tried adding ascorbic acid but nothing happens.
@bumblebeehive2399
@bumblebeehive2399 6 жыл бұрын
Surely a stupid question but at 8.07 and at 8.16 I cannot tell if you are adding water or blowing air into the solution. Is it water or just air or both ?
@astralchemistry8732
@astralchemistry8732 6 жыл бұрын
Not a stupid question. We noticed that it is very hard to tell on the video. Its just synthetic air we blow over the solution in order to facilitate the evaporation process.
@williamiannucci2740
@williamiannucci2740 6 жыл бұрын
Bumblebee Hive . Air to dry it.
@ahmedscrazymixacm1167
@ahmedscrazymixacm1167 4 жыл бұрын
Good job but I was wondering if there is anything that can be used instead of quartz wool or maybe the honey comp of the catalytic converter can be used as it is
@kelvinpino4065
@kelvinpino4065 4 жыл бұрын
No, it's not possible as I already tried that and was a fail, I'm struggling to find the quartz wool
@WaffleStaffel
@WaffleStaffel 3 жыл бұрын
@@kelvinpino4065 I suspect rockwool would be a suitable substitute. In fact the smallest and cheapest quantities of fluffy (non compressed) rockwool on ebay already have _some_ platinum. They're sold as faux gas fireplace embers.
@WaffleStaffel
@WaffleStaffel 3 жыл бұрын
@@kelvinpino4065 I got some wool on ebay once and it shipped from China in a plastic bag, so it was smashed and crushed beyond usefulness. Another reviewer claims it's just glass wool and doesn't stand up to temperature. I haven't tried, but it's awfully coarse.
@kelvinpino4065
@kelvinpino4065 3 жыл бұрын
@@WaffleStaffel I think it depends of the thickness of the fibers of the quartz wool, I got one oz online from a store called whale apparatus in usa, just Google it. I followed all the steps of the video but when I heated the catalyst it became brittle, and had no catalytic properties or is very very low, even it didn't catalize the oxidation of the gas burner, also I tried the former method using hexachloroplatinic acid and ethanol and had the same result. I think that the best way is to directly buy the platinized quartz wool and forget this exhausting process
@WaffleStaffel
@WaffleStaffel 3 жыл бұрын
@@kelvinpino4065 Oh no, I'm sorry it didn't work out. I'll have to check out that source. I hammered some Pt into a flat wire shape and even red hot it wouldn't catalyze butane or propane, but it _did_ work on methanol vapors. Yeah, if you just want the catalyst, buying it on alibaba is probably the way to go. Evidently Pt on kaowool (alumina/silica?) is used as well, so since that's the only thing I can find which stands up to heat without melting or becomin gbrittle, that's the first thing I'm going to try. - www.sciencemadness.org/talk/viewthread.php?tid=13734
@zolt1296
@zolt1296 2 жыл бұрын
Ostwald Oxidation got taken down!! Was using that vid for photography chemistry synthesis from natural materials, can I get a link elsewhere or reupload/file ? Was greatly valuable and now i'm out in the water
@WaffleStaffel
@WaffleStaffel Жыл бұрын
You may check the bitchute channel under the same name.
@arneshbiswas7748
@arneshbiswas7748 3 жыл бұрын
Can Senku borrow some platinum from u to save the world?
@kelvinpino4065
@kelvinpino4065 3 жыл бұрын
Do you have any way to contact you?
@MrBradshawbenjamin
@MrBradshawbenjamin 3 жыл бұрын
Guys, the song is cool, let it be
@DuyNguyen-vf5cv
@DuyNguyen-vf5cv 6 жыл бұрын
platinum seem waste a lot in solution?
@astralchemistry8732
@astralchemistry8732 6 жыл бұрын
A very small amount of platinum is enough to turn the solution deep black. However, the platinum is easily recycled.
@sebandersenwood
@sebandersenwood 6 жыл бұрын
great video, not sure how you got 1mg as an excess of NaCl though. 20mg/195ram=0.1mmol Pt 0.1mmol x 2shoichiometry x 58.5rmmNaCl = 11.7mg NaCl edit: you allso say "0.42 mg of sodium chloridde"
@thesciencefurry
@thesciencefurry 4 ай бұрын
I got hung up on that aswell. I thought my math was wrong. But the 1mg is way too little.
@koukouzee2923
@koukouzee2923 3 жыл бұрын
If I just had the platnium ....or the nitric acid...or a beaker..
@alish5417
@alish5417 3 жыл бұрын
i have bought 5 grams fused quartz wool it cost me 40 dollars 😁
@user-un7sq5bf2d
@user-un7sq5bf2d 2 ай бұрын
الحرارة تضر المحلول!
@jhyland87
@jhyland87 3 жыл бұрын
Great video, all except the unexpectedly annoying and loud music >_
@bertrandschweitzer7020
@bertrandschweitzer7020 6 жыл бұрын
Interesting video but for the love of all that you care about, adjust the volume of that crappy music you use without any kind of logic at 11:20 or so and in some other videos of yours. You go through long stretches of relatively quiet or even silent footage then suddenly, insanely louder techno music destroy your eardrums, especially if you use headphones (I do)...
@k.wanele
@k.wanele 3 жыл бұрын
Im honestly just here to know what the fuck is going on in dr stone
@CatboyChemicalSociety
@CatboyChemicalSociety 3 жыл бұрын
Dr stone plot destroyed. you dont even need Pt to do this experiment and you can use a mix of Mn3O4 and CuO catalyst
@myessyallyahamericus8405
@myessyallyahamericus8405 4 жыл бұрын
Washington dc will be completely leveled to the ground
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